Quarterly Journal of the Chemical Society of London, Part 3, Pages 1153-2704 |
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Page 1582
... acetic acid ( 50 ml . ) was added . The solution was refluxed for a further 1 hr . , concentrated , and treated with aqueous ethanol . The separated product gave yellow needles , m . p . 267 ° ( decomp . ) ( from acetic acid - ethanol ) ...
... acetic acid ( 50 ml . ) was added . The solution was refluxed for a further 1 hr . , concentrated , and treated with aqueous ethanol . The separated product gave yellow needles , m . p . 267 ° ( decomp . ) ( from acetic acid - ethanol ) ...
Page 2390
... acetic acid- chloroform ( 20 ml .; 3 : 1 ) containing a few drops of a 50 % solution of 10N - hydrochloric acid in acetic acid was mixed with chlorine ( 106 mg .: 2.5 mol . ) dissolved in acetic acid- chloroform ( 5 ml .; 3 : 1 ) , and ...
... acetic acid- chloroform ( 20 ml .; 3 : 1 ) containing a few drops of a 50 % solution of 10N - hydrochloric acid in acetic acid was mixed with chlorine ( 106 mg .: 2.5 mol . ) dissolved in acetic acid- chloroform ( 5 ml .; 3 : 1 ) , and ...
Page 2672
... acetic acid ( 20 ml . ) , was hydrogenolysed overnight over 10 % palladium - char- coal ( 3.5 g . ) . Work - up in the usual way gave an oil con- taining acetic acid which could not be removed by evapor- ation . The oil was dissolved in ...
... acetic acid ( 20 ml . ) , was hydrogenolysed overnight over 10 % palladium - char- coal ( 3.5 g . ) . Work - up in the usual way gave an oil con- taining acetic acid which could not be removed by evapor- ation . The oil was dissolved in ...
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Common terms and phrases
absorption acetic acid acetone acetyl adduct alcohol alumina Amer amine anhydride aqueous aromatic ation atom benzene bromide Calc carbon carbonyl CH₂ Chem chloride chloroform chromatography cm.¹ compound cooled crystallised decomp derivative dilute dimethyl distilled doublet dried eluted ester ethanol ethyl acetate evaporated extracted with ether filtered filtrate formed Found fraction gave give heated under reflux hydrochloric acid hydrogen hydrolysis infrared spectrum irradiated isolated isomer ketone light petroleum b. p. lithium aluminium hydride m. p. and mixed methyl ether mixed m. p. mmoles mole multiplet n.m.r. spectrum needles nitrogen obtained oxide phenyl potassium potassium hydroxide prepared protons pyridine quinone reaction mixture reduced pressure reduction requires residue ring room temperature silica gel singlet sodium borohydride sodium hydroxide solution solvent spectra stirred structure sulphuric acid VIII washed yellow yield