Quarterly Journal of the Chemical Society of London |
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Page 3067
... diethyl phosphoro- dithioate gives S - chlorocarbonyl 00 - diethyl phosphorodithioate , a new type of organophosphorus compound , whereas potassium 00 - diethyl phosphoro- thioate gives diethyl phosphorochloridate and tetraethyl ...
... diethyl phosphoro- dithioate gives S - chlorocarbonyl 00 - diethyl phosphorodithioate , a new type of organophosphorus compound , whereas potassium 00 - diethyl phosphoro- thioate gives diethyl phosphorochloridate and tetraethyl ...
Page 3070
... diethyl phosphoro- chloridate and had a spectrum similar to that of S - chlorocarbonyl OO - diethyl phosphoro- dithioate . The product was sealed in soda - glass to await purification by distillation , but decomposed violently after 4 ...
... diethyl phosphoro- chloridate and had a spectrum similar to that of S - chlorocarbonyl OO - diethyl phosphoro- dithioate . The product was sealed in soda - glass to await purification by distillation , but decomposed violently after 4 ...
Page 3074
... diethyl trichloromethylphosphonate is appreciably fast in the absence of peroxidic initiators at 80 ° , although not as fast as the reaction induced by dibenzoyl peroxide or ultraviolet light . In the former case the possibility that ...
... diethyl trichloromethylphosphonate is appreciably fast in the absence of peroxidic initiators at 80 ° , although not as fast as the reaction induced by dibenzoyl peroxide or ultraviolet light . In the former case the possibility that ...
Contents
3082 | 2595 |
Interaction between selenium oxychloride and the trichlorides of boron | 2600 |
NO PAGE | 2601 |
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absorption acetic acid acetic anhydride acetone acetyl added alcohol alkali alumina Amer aqueous ation atom band benzene beryllium boiling bond bromide Calc carbon tetrachloride carbonyl Chem chloride chloroform chromatography cm.¹ colourless complexes compound concentrated cooled crystallised crystals cyclohexanone decomp decomposition derivative diethyl dilute dioxan dissolved distilled elution ester ethanol ethyl acetate evaporated EXPERIMENTAL extracted with ether filtered filtrate formation Found fraction gave heated hydride hydrochloric acid hydrolysis infrared infrared spectrum iodide isolated isomers isorotenolone ketone light petroleum b. p. lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture mole molecule needles nitrate nitric oxide nitrogen obtained peroxide phenyl phosphate potassium precipitate prepared pyridine quinazoline radicals reaction refluxed requires residue room temperature rotenone sample sodium hydroxide solid solution solvent spectra structure sulphate sulphuric acid Table ultraviolet values yellow yield