Quarterly Journal of the Chemical Society of London, Part 4, Pages 3513-4668 |
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Results 1-3 of 79
Page 3676
... Ketone . - o - Aminobenzonitrile ( 9.4 g . ) in dry ether ( 100 ml . ) was added dropwise with stirring to a boiling solution of benzylmagnesium chloride , prepared from benzyl chloride ( 81 g . , 8 mol . ) and magnesium ( 15.4 g . ) in ...
... Ketone . - o - Aminobenzonitrile ( 9.4 g . ) in dry ether ( 100 ml . ) was added dropwise with stirring to a boiling solution of benzylmagnesium chloride , prepared from benzyl chloride ( 81 g . , 8 mol . ) and magnesium ( 15.4 g . ) in ...
Page 3851
... ketone and its hydrate was isolated . Crystallisation of the mixture from light petroleum ( b . p . 60-80 ° ) gave the ketone , and the hydrate ( mixed with some ketone ) as needles , m . p . 75—77 ° ( Found : C , 18-8 ; H , 1-4 ...
... ketone and its hydrate was isolated . Crystallisation of the mixture from light petroleum ( b . p . 60-80 ° ) gave the ketone , and the hydrate ( mixed with some ketone ) as needles , m . p . 75—77 ° ( Found : C , 18-8 ; H , 1-4 ...
Page 3968
... ketones studied with the exception of cyclohexanone , methylpropyl ketone and diisobutyl ketone . From these ketones the products were , respectively , the oxazolidine , an equilibrium mixture of azomethine and oxazolidine , and the ...
... ketones studied with the exception of cyclohexanone , methylpropyl ketone and diisobutyl ketone . From these ketones the products were , respectively , the oxazolidine , an equilibrium mixture of azomethine and oxazolidine , and the ...
Contents
NO PAGE | 3528 |
The adsorption of stearic acid from solution by oxide adsorbents | 3535 |
The effect of pressure of the electrical conductivity of aqueous mixed electrolyte | 3548 |
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Common terms and phrases
absorption acetic acid acetic anhydride acetone acetyl added alcohol alkaline aluminium Amer amine atoms band benzene benzyl boiling bond bromide Calc carbon cations CH₂ chabazite Chem chloride chloroform chromatography cm.¹ colistin compounds concentration constant crystallised crystals decomp derivatives dilute dimethyl dimethylformamide dioxan dissolved distilled dried ester ethanol ether ethyl acetate evaporated extracted filtrate formation formed Found fraction gave give heated hydrochloric acid hydrochloride hydrogen hydrolysis iodide isomer ketone lithium lithium aluminium hydride m. p. and mixed mixed m. p. mixture mole molecules needles nitrate nitric acid nitrogen o-xylene obtained optical oxide oxygen phenyl phosphine picrate polymyxin potassium precipitate prepared prisms proton pyridine reaction recrystallised reduced refluxed requires residue resonance room temperature salt sodium hydroxide solution solvent spectra stirred structure substitution sulphone sulphuric acid Table tetrahydrofuran values washed yellow yield