Quarterly Journal of the Chemical Society of London, Volume 16, Pages 2069-2832

absorption acetic acid acetone added adduct alcohol alumina Amer anhydride aqueous aromatic atom band benzene benzyl boiling bromide Calc carbonate carbonyl carbonyl fluoride CH₂ Chem Chim chloride chloroform chromatography cm.¹ compound cooled crystallised decomp derivatives dimethyl dimethylformamide dissolved distilled dried eluted ester ethanol ether ethyl acetate evaporated extracted with ether ferrocene filtered filtrate fluoride Found fraction gave give heated under reflux hydrochloric acid hydrogen hydrolysis hydroxide i.r. spectrum iodide isolated ketone light petroleum b.p. m.p. and mixed methiodide methyl ether mixed m.p. mixture mmoles mole molecular n.m.r. spectrum needles nitrogen obtained oxidation petroleum phenol piperidine potassium potassium hydroxide prepared protons pyridine reaction rearrangement reduced pressure requires residue ring room temperature silica sodium sodium hydroxide solid solution solvent spectra stirred structure sulphide sulphoxide VIII washed xanthone yellow yield