Quarterly Journal of the Chemical Society of London, Part 3 |
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Page 2375
... 1,3,5 - trinitrobenzene . The trinitro- compound ( 1.3 g . ) in hot benzene ( 5 c.c. ) was added to the distillate ( 1 · 07 g . ) , also in benzene ( 10 c.c. ) , and the solution was heated to the b . p . , diluted with light petroleum ...
... 1,3,5 - trinitrobenzene . The trinitro- compound ( 1.3 g . ) in hot benzene ( 5 c.c. ) was added to the distillate ( 1 · 07 g . ) , also in benzene ( 10 c.c. ) , and the solution was heated to the b . p . , diluted with light petroleum ...
Page 2379
... trinitrobenzene . The variation can only be explained if the primary complex ionises . The electrical conductivity of mixtures of 1,3,5 - trinitrobenzene with N - ethylaniline or NN- diethylaniline in ethanol differed little from that ...
... trinitrobenzene . The variation can only be explained if the primary complex ionises . The electrical conductivity of mixtures of 1,3,5 - trinitrobenzene with N - ethylaniline or NN- diethylaniline in ethanol differed little from that ...
Page 2383
... 1,3,5 - trinitrobenzene- diethylamine in ethanol as it is for pyridine solutions of 1,3,5 - trinitrobenzene . Equilibrium measurements on the former system agree well with those to be expected if a 1 : 1 complex were formed . That the ...
... 1,3,5 - trinitrobenzene- diethylamine in ethanol as it is for pyridine solutions of 1,3,5 - trinitrobenzene . Equilibrium measurements on the former system agree well with those to be expected if a 1 : 1 complex were formed . That the ...
Contents
ABEL E W Bennett M A and Wilkinson G | 2323 |
Bourne E J Hartigan J and Weigel H | 2332 |
Clark E R | 2344 |
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1,3,5-trinitrobenzene absorption acetic acid acetic anhydride acetone added alcohol alkaline alkyl Amer amine ammonia anhydride atom benzene boiling bond bromide Calc carbon Chem chloride chloroform chromatography complex compound concentration constant cooled crystallised crystals curve decomp derivatives diethylamine dilute dimer dioxan dioxide dissolved distilled dried eluted ester ethanol evaporated filtered filtrate formation formed Found fraction gave give glycollic acid glyoxylic acid heated hydride hydrochloric acid hydrolysis hydroxide infrared infrared spectrum iodide isolated isomer K₁ light petroleum b. p. lithium lithium aluminium hydride m. p. and mixed methyl methyl iodide mixed m. p. mixture mole molecular molecule nitrogen obtained oxidation oxygen perchlorate picrate polymer potassium precipitate prepared prisms pyridine reaction reduced refluxed requires residue room temperature salt sodium hydroxide solid solvent spectra stirred structure sulphuric acid Table titration ultraviolet values washed yield