Quarterly Journal of the Chemical Society of London, Part 3 |
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Results 1-3 of 82
Page 2424
... alcohol - benzene ) , m . p . 114.5-116 ° ( 115 ° 9 ) ( 90 % ) . N - Methyl - 2 4 : 6 - trinitroaniline , yellow needles ( from alcohol ) , m . p . 114-115 ° ( 113-114 ° 9 ) ( 95 % ) . N - Methyl - 2 : 4 : 6 - trinitro - N ...
... alcohol - benzene ) , m . p . 114.5-116 ° ( 115 ° 9 ) ( 90 % ) . N - Methyl - 2 4 : 6 - trinitroaniline , yellow needles ( from alcohol ) , m . p . 114-115 ° ( 113-114 ° 9 ) ( 95 % ) . N - Methyl - 2 : 4 : 6 - trinitro - N ...
Page 2907
... alcohol reduction , and n , 20 1.4620 , from reduction in alkali ( Found : C , 74-8 ; H , 12-6 ; and C , 75 · 0 ; H , 12.5 ; respectively . Calc . for CHO : C , 75-0 ; H , 12.5 % ) gave the same infrared spectra . Wallach 34 gives n20 ...
... alcohol reduction , and n , 20 1.4620 , from reduction in alkali ( Found : C , 74-8 ; H , 12-6 ; and C , 75 · 0 ; H , 12.5 ; respectively . Calc . for CHO : C , 75-0 ; H , 12.5 % ) gave the same infrared spectra . Wallach 34 gives n20 ...
Page 2935
... alcohol ( 50 ml . ) was added , and the mixture was vigorously shaken for 15 min . and kept for 2 hr . The resulting white precipitate was filtered off , washed with saturated potassium iodide solution , then several times with water ...
... alcohol ( 50 ml . ) was added , and the mixture was vigorously shaken for 15 min . and kept for 2 hr . The resulting white precipitate was filtered off , washed with saturated potassium iodide solution , then several times with water ...
Contents
ABEL E W Bennett M A and Wilkinson G | 2323 |
Bourne E J Hartigan J and Weigel H | 2332 |
Clark E R | 2344 |
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1,3,5-trinitrobenzene absorption acetic acid acetic anhydride acetone added alcohol alkaline alkyl Amer amine ammonia anhydride atom benzene boiling bond bromide Calc carbon Chem chloride chloroform chromatography complex compound concentration constant cooled crystallised crystals curve decomp derivatives diethylamine dilute dimer dioxan dioxide dissolved distilled dried eluted ester ethanol evaporated filtered filtrate formation formed Found fraction gave give glycollic acid glyoxylic acid heated hydride hydrochloric acid hydrolysis hydroxide infrared infrared spectrum iodide isolated isomer K₁ light petroleum b. p. lithium lithium aluminium hydride m. p. and mixed methyl methyl iodide mixed m. p. mixture mole molecular molecule nitrogen obtained oxidation oxygen perchlorate picrate polymer potassium precipitate prepared prisms pyridine reaction reduced refluxed requires residue room temperature salt sodium hydroxide solid solvent spectra stirred structure sulphuric acid Table titration ultraviolet values washed yield