Quarterly Journal of the Chemical Society of London, Part 3 |
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Page 2528
... hydroxide , and thence into the other salts required , as follows . The Grignard reagent from s - butyl bromide ( 100 g . ) in ether ( 300 ml . ) was added to finely powdered mercuric bromide ( 300 g . ) suspended in ether ( 250 ml ...
... hydroxide , and thence into the other salts required , as follows . The Grignard reagent from s - butyl bromide ( 100 g . ) in ether ( 300 ml . ) was added to finely powdered mercuric bromide ( 300 g . ) suspended in ether ( 250 ml ...
Page 2834
... hydroxide . Dihydrogeodoxin ( 100 mg . ) was refluxed with ethanol ( 15 c.c. ) and N - sodium hydroxide ( 7.5 c.c. ) for 1 hr . Acidification followed by removal of ethanol under reduced pressure afforded a precipitate ( 100 mg ...
... hydroxide . Dihydrogeodoxin ( 100 mg . ) was refluxed with ethanol ( 15 c.c. ) and N - sodium hydroxide ( 7.5 c.c. ) for 1 hr . Acidification followed by removal of ethanol under reduced pressure afforded a precipitate ( 100 mg ...
Page 3043
... hydroxide solution was evaporated to dryness on the water - bath , and the residue boiled with chloroform ( 750 ml . ) and filtered . The residue after evaporation of the filtrate was dissolved in 3N - sodium hydroxide from which 1 ...
... hydroxide solution was evaporated to dryness on the water - bath , and the residue boiled with chloroform ( 750 ml . ) and filtered . The residue after evaporation of the filtrate was dissolved in 3N - sodium hydroxide from which 1 ...
Contents
ABEL E W Bennett M A and Wilkinson G | 2323 |
Bourne E J Hartigan J and Weigel H | 2332 |
Clark E R | 2344 |
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1,3,5-trinitrobenzene absorption acetic acid acetic anhydride acetone added alcohol alkaline alkyl Amer amine ammonia anhydride atom benzene boiling bond bromide Calc carbon Chem chloride chloroform chromatography complex compound concentration constant cooled crystallised crystals curve decomp derivatives diethylamine dilute dimer dioxan dioxide dissolved distilled dried eluted ester ethanol evaporated filtered filtrate formation formed Found fraction gave give glycollic acid glyoxylic acid heated hydride hydrochloric acid hydrolysis hydroxide infrared infrared spectrum iodide isolated isomer K₁ light petroleum b. p. lithium lithium aluminium hydride m. p. and mixed methyl methyl iodide mixed m. p. mixture mole molecular molecule nitrogen obtained oxidation oxygen perchlorate picrate polymer potassium precipitate prepared prisms pyridine reaction reduced refluxed requires residue room temperature salt sodium hydroxide solid solvent spectra stirred structure sulphuric acid Table titration ultraviolet values washed yield