Quarterly Journal of the Chemical Society of London |
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Page 215
... ( Calc .: 274 ) . - = Octamethyl ester . M. p . 141 ° ( 139 ° ) ( Found : C , 48-35 ; H , 4.85 ; M , by vapour - pressure equilibration of a benzene solution against olive oil , 54030 ; cryoscopically in benzene , 530 ± 30. Calc . for ...
... ( Calc .: 274 ) . - = Octamethyl ester . M. p . 141 ° ( 139 ° ) ( Found : C , 48-35 ; H , 4.85 ; M , by vapour - pressure equilibration of a benzene solution against olive oil , 54030 ; cryoscopically in benzene , 530 ± 30. Calc . for ...
Page 802
... calc . Indices . F , obs . F , calc . Indices . F , obs . F , calc , Indices . F , obs . F , calc . 1010 34 40 8080 12 18 7180 17 14 4370 16 7 2020 28 31 1120 19 22 2240 74 83 5380 0 4 3030 15 -7 2130 16 6 3250 16 18 4480 41 37 4040 26 ...
... calc . Indices . F , obs . F , calc . Indices . F , obs . F , calc , Indices . F , obs . F , calc . 1010 34 40 8080 12 18 7180 17 14 4370 16 7 2020 28 31 1120 19 22 2240 74 83 5380 0 4 3030 15 -7 2130 16 6 3250 16 18 4480 41 37 4040 26 ...
Page 856
... ( Calc . for C , H , N , HC1 : 3.85 g . ) ( Found : Cl , 29-2 . Calc .: Cl , 30.8 % ) . The ethereal solution was poured on ice , washed with a minimum amount of solution of sodium carbonate , dried ( sodium sulphate ) and evaporated ...
... ( Calc . for C , H , N , HC1 : 3.85 g . ) ( Found : Cl , 29-2 . Calc .: Cl , 30.8 % ) . The ethereal solution was poured on ice , washed with a minimum amount of solution of sodium carbonate , dried ( sodium sulphate ) and evaporated ...
Contents
An Investigation of the Occurrence of the Coordinate or Dative Link by Electric Dipolemoment | 38 |
Electrolytic Dissociation Processes Part IV The Ionisation of a CarbonHalogen Bond | 129 |
By J SHERIDAN | 133 |
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Common terms and phrases
4-benzthiazine absorption acetic anhydride acetone acetyl acetylene added addition adsorbed alkali Amer ammonia aqueous atoms benzene boiling bond Calc carbinol carbon catalyst CH₂ Chem chloroform colourless needles compound concentrated condensation cooling crystallised from alcohol crystals cyclisation D.Sc decomp derivative described dilute dissolved distilled dried ester ethanol ether ethylene evaporated EXPERIMENTAL extracted filtered filtrate formation formed Found fraction gave give heated hydrocarbons hydrochloric acid hydrogen bromide hydrogen chloride hydrolysis iodide isolated ketone light petroleum liquid methiodide method methyl alcohol mixed m. p. mixture molecule nickel nitric nitrogen obtained optically oxide oxychloride phosphate phosphorus picrate potassium potassium hydroxide precipitate prepared pressure prisms pyridine reaction reduced refluxed requires residue ring room temperature salt saturated separated sodium carbonate sodium hydroxide solid soluble solution solvent structure substance sulphate sulphuric acid vacuum washed yellow needles yield zinc