Quarterly Journal of the Chemical Society of London |
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Page 107
... oxychloride , or of the tri - ester and oxychloride , were essentially phosphorus compounds , probably mixed with pyridine hydrochloride , and resulted from the interaction of pyridine with the products of reactions that had already ...
... oxychloride , or of the tri - ester and oxychloride , were essentially phosphorus compounds , probably mixed with pyridine hydrochloride , and resulted from the interaction of pyridine with the products of reactions that had already ...
Page 110
... oxychloride ( 2 mols . ) were mixed and kept at 15 ° / 13 mm . for 9 hours , and the product ( Found : Cl , 34.8 % ) when treated with pyridine ( 2 · 0 g . ) in ethereal solution gave a precipitate ( 4 · 38 g . ) ( Found : Ĉl , 21-7 ; P ...
... oxychloride ( 2 mols . ) were mixed and kept at 15 ° / 13 mm . for 9 hours , and the product ( Found : Cl , 34.8 % ) when treated with pyridine ( 2 · 0 g . ) in ethereal solution gave a precipitate ( 4 · 38 g . ) ( Found : Ĉl , 21-7 ; P ...
Page 111
... oxychloride ( 3 mols . ) at 0 ° for 4 hours , ( + ) a - chloroethylbenzene ( 1 · 7 g . ) , ab6 ° + 4 · 6 ° , and a residue ( 1 · 2 g . ) were formed . Interaction of ( - ) Phenylmethylcarbinol and Phosphorus Oxychloride in the Presence ...
... oxychloride ( 3 mols . ) at 0 ° for 4 hours , ( + ) a - chloroethylbenzene ( 1 · 7 g . ) , ab6 ° + 4 · 6 ° , and a residue ( 1 · 2 g . ) were formed . Interaction of ( - ) Phenylmethylcarbinol and Phosphorus Oxychloride in the Presence ...
Contents
An Investigation of the Occurrence of the Coordinate or Dative Link by Electric Dipolemoment | 38 |
Electrolytic Dissociation Processes Part IV The Ionisation of a CarbonHalogen Bond | 129 |
By J SHERIDAN | 133 |
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Common terms and phrases
4-benzthiazine absorption acetic anhydride acetone acetyl acetylene added addition adsorbed alkali Amer ammonia aqueous atoms benzene boiling bond Calc carbinol carbon catalyst CH₂ Chem chloroform colourless needles compound concentrated condensation cooling crystallised from alcohol crystals cyclisation D.Sc decomp derivative described dilute dissolved distilled dried ester ethanol ether ethylene evaporated EXPERIMENTAL extracted filtered filtrate formation formed Found fraction gave give heated hydrocarbons hydrochloric acid hydrogen bromide hydrogen chloride hydrolysis iodide isolated ketone light petroleum liquid methiodide method methyl alcohol mixed m. p. mixture molecule nickel nitric nitrogen obtained optically oxide oxychloride phosphate phosphorus picrate potassium potassium hydroxide precipitate prepared pressure prisms pyridine reaction reduced refluxed requires residue ring room temperature salt saturated separated sodium carbonate sodium hydroxide solid soluble solution solvent structure substance sulphate sulphuric acid vacuum washed yellow needles yield zinc