Quarterly Journal of the Chemical Society of London |
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Results 1-3 of 72
Page 109
... residue ( 0.45 g . ) ; and from the carbonate solution , a residue ( 0-4 g . ) ( Found : P , 12 · 3 % ) . 18 ( 3 ) From oxychloride ( 1 mol . ) , and 1 hour's standing at 15 ° / 15 mm . , there resulted ( - ) 8 - octyl chloride ( 1.05 g ...
... residue ( 0.45 g . ) ; and from the carbonate solution , a residue ( 0-4 g . ) ( Found : P , 12 · 3 % ) . 18 ( 3 ) From oxychloride ( 1 mol . ) , and 1 hour's standing at 15 ° / 15 mm . , there resulted ( - ) 8 - octyl chloride ( 1.05 g ...
Page 856
... residue was obtained , and only part of this was volatile . It appears from these results that the phosphite formed during the addition of the first third of the trichloride is converted into a mixture of the dichlorophosphite and ...
... residue was obtained , and only part of this was volatile . It appears from these results that the phosphite formed during the addition of the first third of the trichloride is converted into a mixture of the dichlorophosphite and ...
Page 857
... residue was heated up to 110 ° / 15 mm .; there was a ace of distillate at 50 ° / 15 mm . , and the final residue was weighed and examined . From the appropriate results which e recorded below , the residues appear to be specimens of ...
... residue was heated up to 110 ° / 15 mm .; there was a ace of distillate at 50 ° / 15 mm . , and the final residue was weighed and examined . From the appropriate results which e recorded below , the residues appear to be specimens of ...
Contents
An Investigation of the Occurrence of the Coordinate or Dative Link by Electric Dipolemoment | 38 |
Electrolytic Dissociation Processes Part IV The Ionisation of a CarbonHalogen Bond | 129 |
By J SHERIDAN | 133 |
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Common terms and phrases
4-benzthiazine absorption acetic anhydride acetone acetyl acetylene added addition adsorbed alkali Amer ammonia aqueous atoms benzene boiling bond Calc carbinol carbon catalyst CH₂ Chem chloroform colourless needles compound concentrated condensation cooling crystallised from alcohol crystals cyclisation D.Sc decomp derivative described dilute dissolved distilled dried ester ethanol ether ethylene evaporated EXPERIMENTAL extracted filtered filtrate formation formed Found fraction gave give heated hydrocarbons hydrochloric acid hydrogen bromide hydrogen chloride hydrolysis iodide isolated ketone light petroleum liquid methiodide method methyl alcohol mixed m. p. mixture molecule nickel nitric nitrogen obtained optically oxide oxychloride phosphate phosphorus picrate potassium potassium hydroxide precipitate prepared pressure prisms pyridine reaction reduced refluxed requires residue ring room temperature salt saturated separated sodium carbonate sodium hydroxide solid soluble solution solvent structure substance sulphate sulphuric acid vacuum washed yellow needles yield zinc