Quarterly Journal of the Chemical Society of London |
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Page 110
Chemical Society (Great Britain). together with the ethereal washings of the solid afforded , after aqueous treatment , octylene and ( - ) ẞ - octyl chloride ( 0.55 g . ) , b . p . 59 ° / 13 mm . , a18 ° -27.9 ° . The solid was not a ...
Chemical Society (Great Britain). together with the ethereal washings of the solid afforded , after aqueous treatment , octylene and ( - ) ẞ - octyl chloride ( 0.55 g . ) , b . p . 59 ° / 13 mm . , a18 ° -27.9 ° . The solid was not a ...
Page 663
... solid material . Recrystallisation of the combined solid fractions gave N - benzyl - N- methylmorpholinium chloride , m . p . 236 ° ( decomp . ) after shrinking at 230 ° ( Found : Cl , 15.6 . C12H1ONCI requires Cl , 15.6 % ) . The ...
... solid material . Recrystallisation of the combined solid fractions gave N - benzyl - N- methylmorpholinium chloride , m . p . 236 ° ( decomp . ) after shrinking at 230 ° ( Found : Cl , 15.6 . C12H1ONCI requires Cl , 15.6 % ) . The ...
Page 867
... solid sodium hydroxide in a vacuum desiccator . The resulting crude yellowish solid ( 14 g . , 62 % ) consisted of a - chloroethylidene acetamidine hydrochloride and , after washing with dry ether , had m . p . 78 ° . It was not further ...
... solid sodium hydroxide in a vacuum desiccator . The resulting crude yellowish solid ( 14 g . , 62 % ) consisted of a - chloroethylidene acetamidine hydrochloride and , after washing with dry ether , had m . p . 78 ° . It was not further ...
Contents
An Investigation of the Occurrence of the Coordinate or Dative Link by Electric Dipolemoment | 38 |
Electrolytic Dissociation Processes Part IV The Ionisation of a CarbonHalogen Bond | 129 |
By J SHERIDAN | 133 |
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Common terms and phrases
4-benzthiazine absorption acetic anhydride acetone acetyl acetylene added addition adsorbed alkali Amer ammonia aqueous atoms benzene boiling bond Calc carbinol carbon catalyst CH₂ Chem chloroform colourless needles compound concentrated condensation cooling crystallised from alcohol crystals cyclisation D.Sc decomp derivative described dilute dissolved distilled dried ester ethanol ether ethylene evaporated EXPERIMENTAL extracted filtered filtrate formation formed Found fraction gave give heated hydrocarbons hydrochloric acid hydrogen bromide hydrogen chloride hydrolysis iodide isolated ketone light petroleum liquid methiodide method methyl alcohol mixed m. p. mixture molecule nickel nitric nitrogen obtained optically oxide oxychloride phosphate phosphorus picrate potassium potassium hydroxide precipitate prepared pressure prisms pyridine reaction reduced refluxed requires residue ring room temperature salt saturated separated sodium carbonate sodium hydroxide solid soluble solution solvent structure substance sulphate sulphuric acid vacuum washed yellow needles yield zinc