Journal of the Chemical SocietyThe Society., 1949 |
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Results 1-3 of 78
Page 924
... ( Found : Pb , 50-5 . C12H2O , Pb requires Pb , 50.8 % ) . Tri - n - propyl - lead Bromide . - An aqueous solution of tri - n - propyl - lead hydroxide was added to dilute hydrobromic acid until neutral . After standing for 30 minutes ...
... ( Found : Pb , 50-5 . C12H2O , Pb requires Pb , 50.8 % ) . Tri - n - propyl - lead Bromide . - An aqueous solution of tri - n - propyl - lead hydroxide was added to dilute hydrobromic acid until neutral . After standing for 30 minutes ...
Page 1167
... ( Found : S , 13.1 % ) . The precipitate obtained by acidifying the alkaline solution was stirred for 1 hour with 10 % potassium hydrogen carbonate solution ( to remove benzoic acid ) , and the insoluble triazole collected and ...
... ( Found : S , 13.1 % ) . The precipitate obtained by acidifying the alkaline solution was stirred for 1 hour with 10 % potassium hydrogen carbonate solution ( to remove benzoic acid ) , and the insoluble triazole collected and ...
Page 1313
... ( Found : C , 67-5 ; H , 7-7 . CHON requires C , 67-5 ; H , 7.6 % ) ; hydro- chloride , rhombic prisms , m . p . 200-201 ° ( previous softening ) from 2N - hydrochloric acid ( Found : Cl , 12-4 ; equiv . , 284-6 . CH20ONCI requires Cl ...
... ( Found : C , 67-5 ; H , 7-7 . CHON requires C , 67-5 ; H , 7.6 % ) ; hydro- chloride , rhombic prisms , m . p . 200-201 ° ( previous softening ) from 2N - hydrochloric acid ( Found : Cl , 12-4 ; equiv . , 284-6 . CH20ONCI requires Cl ...
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4-dinitrophenylhydrazone absorption acetic anhydride acetone acetyl acidified added aldehyde alkaline aluminium chloride Amer amine ammonia aniline aqueous sodium atom benzene boiling bromine Calc carbon catalyst CH₂ Chem chloroform citrinin colourless needles compound condensation containing cooled crystallised crystallised from alcohol crystals cyanide cyclisation decomp derivative dilute dissolved distilled dried electrode ester evaporated extracted with ether filtered filtrate formed colourless Found fraction gave give heated under reflux hydrochloric acid hydrogen chloride hydrolysis iodide isolated ketone lactone light petroleum b. p. m. p. and mixed methanol method methyl alcohol minutes mixed m. p. mixture molecule obtained oxide phenol phosphoric picrate potassium hydroxide precipitate prepared pyridine reaction reduced pressure requires residue resin room temperature salt separated sodium hydroxide solid soluble solution solvent specimen structure substance sulphuric acid triethylamine values washed yellow needles yield