Journal of the Chemical SocietyThe Society., 1949 |
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Results 1-3 of 69
Page 1157
... evaporated under reduced pressure at 80 ° , and the solid residue was crystallised from alcohol , giving semicarbazide ( 24 g . ) , m . p . 96 ° , undepressed on admixture with an authentic specimen ( Found : C , 16-2 ; H , 6 · 6 ; N ...
... evaporated under reduced pressure at 80 ° , and the solid residue was crystallised from alcohol , giving semicarbazide ( 24 g . ) , m . p . 96 ° , undepressed on admixture with an authentic specimen ( Found : C , 16-2 ; H , 6 · 6 ; N ...
Page 1363
... evaporated to dryness under diminished pressure . residue was dissolved in methyl alcohol , filtered , and ether added . The methylglucofuranoside Calc . for C , H1207 : OMe , 5 : 6 - carbonate separated , and was filtered off and ...
... evaporated to dryness under diminished pressure . residue was dissolved in methyl alcohol , filtered , and ether added . The methylglucofuranoside Calc . for C , H1207 : OMe , 5 : 6 - carbonate separated , and was filtered off and ...
Page 1623
... evaporate . Dry air was blown through the flask for 2 hours , the residue dried over phosphoric oxide and extracted with ether , the extract evaporated , and the product distilled as above . The yield was 1.6 g . ( Found : C , 66-0 ; H ...
... evaporate . Dry air was blown through the flask for 2 hours , the residue dried over phosphoric oxide and extracted with ether , the extract evaporated , and the product distilled as above . The yield was 1.6 g . ( Found : C , 66-0 ; H ...
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Common terms and phrases
4-dinitrophenylhydrazone absorption acetic anhydride acetone acetyl acidified added aldehyde alkaline aluminium chloride Amer amine ammonia aniline aqueous sodium atom benzene boiling bromine Calc carbon catalyst CH₂ Chem chloroform citrinin colourless needles compound condensation containing cooled crystallised crystallised from alcohol crystals cyanide cyclisation decomp derivative dilute dissolved distilled dried electrode ester evaporated extracted with ether filtered filtrate formed colourless Found fraction gave give heated under reflux hydrochloric acid hydrogen chloride hydrolysis iodide isolated ketone lactone light petroleum b. p. m. p. and mixed methanol method methyl alcohol minutes mixed m. p. mixture molecule obtained oxide phenol phosphoric picrate potassium hydroxide precipitate prepared pyridine reaction reduced pressure requires residue resin room temperature salt separated sodium hydroxide solid soluble solution solvent specimen structure substance sulphuric acid triethylamine values washed yellow needles yield