Journal of the Chemical SocietyThe Society., 1949 |
From inside the book
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Page 819
... salt , crystallising from water in colourless needles ( Found : Ag , 28-8 . C13H12O , PAg requires Ag , 29.0 % ) . Catalytic hydrogenation of the free acid ester regenerated from the cyclohexylamine salt yielded phenyl dihydrogen ...
... salt , crystallising from water in colourless needles ( Found : Ag , 28-8 . C13H12O , PAg requires Ag , 29.0 % ) . Catalytic hydrogenation of the free acid ester regenerated from the cyclohexylamine salt yielded phenyl dihydrogen ...
Page 921
... salt . The removal of any unchanged trialkyl - lead chloride often presents a difficulty here . A useful variation ( 3 ) is to use the silver salt , but this is unsuitable for large - scale work . The method of widest application ( 4 ) ...
... salt . The removal of any unchanged trialkyl - lead chloride often presents a difficulty here . A useful variation ( 3 ) is to use the silver salt , but this is unsuitable for large - scale work . The method of widest application ( 4 ) ...
Page 1183
... salt crystallised from a 1 : 1 mixture of chloroform and alcohol , and after repeated recrystallisation from the same solvent the optically pure strychnine ( + ) - acid salt , [ x ] 291 + 69-7 ° and [ x ] + 80 · 7 ° in chloroform , was ...
... salt crystallised from a 1 : 1 mixture of chloroform and alcohol , and after repeated recrystallisation from the same solvent the optically pure strychnine ( + ) - acid salt , [ x ] 291 + 69-7 ° and [ x ] + 80 · 7 ° in chloroform , was ...
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Common terms and phrases
4-dinitrophenylhydrazone absorption acetic anhydride acetone acetyl acidified added aldehyde alkaline aluminium chloride Amer amine ammonia aniline aqueous sodium atom benzene boiling bromine Calc carbon catalyst CH₂ Chem chloroform citrinin colourless needles compound condensation containing cooled crystallised crystallised from alcohol crystals cyanide cyclisation decomp derivative dilute dissolved distilled dried electrode ester evaporated extracted with ether filtered filtrate formed colourless Found fraction gave give heated under reflux hydrochloric acid hydrogen chloride hydrolysis iodide isolated ketone lactone light petroleum b. p. m. p. and mixed methanol method methyl alcohol minutes mixed m. p. mixture molecule obtained oxide phenol phosphoric picrate potassium hydroxide precipitate prepared pyridine reaction reduced pressure requires residue resin room temperature salt separated sodium hydroxide solid soluble solution solvent specimen structure substance sulphuric acid triethylamine values washed yellow needles yield