Journal of the Chemical SocietyThe Society., 1949 |
From inside the book
Results 1-3 of 79
Page 912
... yellow needles , m . p . 248 ° ( Found : C , 47-5 ; H , 2 · 6 ; N , 6 · 5 . C16H10ON , Br , requires C , 47.3 ; H , 2.5 ; N , 6 · 9 % ) . ( b ) A mixture of phenylglyoxal ( 4 · 02 g . ) and ammonium formate ( 11.3 g . ) was heated to ...
... yellow needles , m . p . 248 ° ( Found : C , 47-5 ; H , 2 · 6 ; N , 6 · 5 . C16H10ON , Br , requires C , 47.3 ; H , 2.5 ; N , 6 · 9 % ) . ( b ) A mixture of phenylglyoxal ( 4 · 02 g . ) and ammonium formate ( 11.3 g . ) was heated to ...
Page 1017
... yellow , fluffy needles ( 2 ) ( yield , 98 % ) ( Found : C , 54.4 ; H , 3.05 ; N , 22.8 . CH , O , N , requires C , 54.0 ; H , 2-9 ; N , 22.5 % ) . The 7 - nitro- isomer separated ( 1 or 2 ) in stout , yellow , brittle needles , m . p ...
... yellow , fluffy needles ( 2 ) ( yield , 98 % ) ( Found : C , 54.4 ; H , 3.05 ; N , 22.8 . CH , O , N , requires C , 54.0 ; H , 2-9 ; N , 22.5 % ) . The 7 - nitro- isomer separated ( 1 or 2 ) in stout , yellow , brittle needles , m . p ...
Page 1534
... yellow precipitate was crystallised from aqueous ethanol ( charcoal ) and then acetic acid ; glittering yellow needles , m . p . 239-240 ° ( decomp . ) ( Found : N , 5-8 Cl , 14-25 . C11H , O , NCI requires N , 5 · 55 ; Cl , 14 · 1 ...
... yellow precipitate was crystallised from aqueous ethanol ( charcoal ) and then acetic acid ; glittering yellow needles , m . p . 239-240 ° ( decomp . ) ( Found : N , 5-8 Cl , 14-25 . C11H , O , NCI requires N , 5 · 55 ; Cl , 14 · 1 ...
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Common terms and phrases
4-dinitrophenylhydrazone absorption acetic anhydride acetone acetyl acidified added aldehyde alkaline aluminium chloride Amer amine ammonia aniline aqueous sodium atom benzene boiling bromine Calc carbon catalyst CH₂ Chem chloroform citrinin colourless needles compound condensation containing cooled crystallised crystallised from alcohol crystals cyanide cyclisation decomp derivative dilute dissolved distilled dried electrode ester evaporated extracted with ether filtered filtrate formed colourless Found fraction gave give heated under reflux hydrochloric acid hydrogen chloride hydrolysis iodide isolated ketone lactone light petroleum b. p. m. p. and mixed methanol method methyl alcohol minutes mixed m. p. mixture molecule obtained oxide phenol phosphoric picrate potassium hydroxide precipitate prepared pyridine reaction reduced pressure requires residue resin room temperature salt separated sodium hydroxide solid soluble solution solvent specimen structure substance sulphuric acid triethylamine values washed yellow needles yield