Journal of the Chemical SocietyThe Society., 1949 |
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Page 1017
... ( yield , 95 % ) ( Found : C , 53-9 ; H , 3.0 ; N , 22.3 % ) 6 - Nitro - 4-6 ' - methyl - 3 ' - quinolylaminoquinazoline crystallised ( 1 ) in warts of fine , deep yellow needles , m . p . 294-295 ° ( yield , 100 % ) ( Found : C , 65-8 ...
... ( yield , 95 % ) ( Found : C , 53-9 ; H , 3.0 ; N , 22.3 % ) 6 - Nitro - 4-6 ' - methyl - 3 ' - quinolylaminoquinazoline crystallised ( 1 ) in warts of fine , deep yellow needles , m . p . 294-295 ° ( yield , 100 % ) ( Found : C , 65-8 ...
Page 1122
... yield was 13 % ( Found : Cl , 5 · 45 . C34H0O2NCIS , requires Cl , 5 · 3 % ) . The dark green crystals had m . p . 174 ° ( decomp . ) . The broad absorption curve had its maximum at 5180 a . The dye decreased the normal photographic ...
... yield was 13 % ( Found : Cl , 5 · 45 . C34H0O2NCIS , requires Cl , 5 · 3 % ) . The dark green crystals had m . p . 174 ° ( decomp . ) . The broad absorption curve had its maximum at 5180 a . The dye decreased the normal photographic ...
Page 1130
... yield . After another such recrystallisation , the yield was 41 % ( Found , after drying in a vacuum at 60-80 ° : S , 22.3 . C12H1O , NS , requires S , 22.55 % ) . The yellow powder had m . p . 169 ° . The absorption maximum was at 4575 ...
... yield . After another such recrystallisation , the yield was 41 % ( Found , after drying in a vacuum at 60-80 ° : S , 22.3 . C12H1O , NS , requires S , 22.55 % ) . The yellow powder had m . p . 169 ° . The absorption maximum was at 4575 ...
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Common terms and phrases
4-dinitrophenylhydrazone absorption acetic anhydride acetone acetyl acidified added aldehyde alkaline aluminium chloride Amer amine ammonia aniline aqueous sodium atom benzene boiling bromine Calc carbon catalyst CH₂ Chem chloroform citrinin colourless needles compound condensation containing cooled crystallised crystallised from alcohol crystals cyanide cyclisation decomp derivative dilute dissolved distilled dried electrode ester evaporated extracted with ether filtered filtrate formed colourless Found fraction gave give heated under reflux hydrochloric acid hydrogen chloride hydrolysis iodide isolated ketone lactone light petroleum b. p. m. p. and mixed methanol method methyl alcohol minutes mixed m. p. mixture molecule obtained oxide phenol phosphoric picrate potassium hydroxide precipitate prepared pyridine reaction reduced pressure requires residue resin room temperature salt separated sodium hydroxide solid soluble solution solvent specimen structure substance sulphuric acid triethylamine values washed yellow needles yield