Journal of the Chemical SocietyThe Society., 1958 |
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Page 1512
... hydrochloric acid ( 45 ml . ) until the solids had dissolved and then for a further 30 min . , yielding prismatic ... hydrochloric acid . ( g ) 5 - n - Hexyloxycarbonylamino - 1 3 : 4 - thiadiazole - 2 - sulphonamide ( 4 g . ) was ...
... hydrochloric acid ( 45 ml . ) until the solids had dissolved and then for a further 30 min . , yielding prismatic ... hydrochloric acid . ( g ) 5 - n - Hexyloxycarbonylamino - 1 3 : 4 - thiadiazole - 2 - sulphonamide ( 4 g . ) was ...
Page 1579
... hydrochloric acid , the solid was filtered off and washed with dilute hydrochloric acid and water . y - Coronenylbutyric acid formed flat pale yellow needles ( 1.35 g . ) , m . p . 277–287 ° ( decomp . ) ( from xylene ) , which ...
... hydrochloric acid , the solid was filtered off and washed with dilute hydrochloric acid and water . y - Coronenylbutyric acid formed flat pale yellow needles ( 1.35 g . ) , m . p . 277–287 ° ( decomp . ) ( from xylene ) , which ...
Page 1858
... hydrochloric acid . A mixture of bromine ( 500 g . ) , water ( 112 c.c. ) , and concentrated hydrochloric acid ( 112 c.c. ) was added during 24 hr . to a stirred suspension of pseudocumene - 5 - sulphonic acid ( from 360 g . of pseudo ...
... hydrochloric acid . A mixture of bromine ( 500 g . ) , water ( 112 c.c. ) , and concentrated hydrochloric acid ( 112 c.c. ) was added during 24 hr . to a stirred suspension of pseudocumene - 5 - sulphonic acid ( from 360 g . of pseudo ...
Contents
1715 | 1310 |
The kinetics of the hydrolysis of methylene dichloride | 1326 |
Firstorder calculation of factor group splittings in the electronic spectra of durene | 1347 |
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acetic acid acetic anhydride acetone added alcohol alkaline Amer ammonia anhydride aqueous methanol atom band benzene boiling bromide Calc CH₂ Chem chloroform chromatography colourless complex compound concentration constant cooled crystallised crystals decomp derivative dichloride dilute dimethyl dioxan dissolved distilled dried eluted ergoflavin ester ethanol ethyl acetate evaporated EXPERIMENTAL filtered filtrate formed Found fraction gallium gave give H₂O heated hydrochloric acid hydrogen chloride hydrolysis iodide ionisation isolated ketone light petroleum b. p. lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture mole mole-¹ molecular molecule nitrogen obtained oxidation peroxide phenyl phosphate picrate potassium potassium hydroxide precipitate prepared prisms pyridine reaction reduced refluxed requires residue room temperature salt sodium hydroxide solid solution solvent spectra structure sulphuric acid synthesis Table trisaccharide ultraviolet values washed yellow needles yield zinc chloride