Quarterly Journal of the Chemical Society of London |
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Page 115
... gives pure tert . - butyl hypochlorite , b.p. 77—79 ° ( 65 g . , 60 % ) . We are indebted to the Chief Scientific ... give the required acetyl compound , and a product was isolated which proved to be the diacetyl derivative . Later , it ...
... gives pure tert . - butyl hypochlorite , b.p. 77—79 ° ( 65 g . , 60 % ) . We are indebted to the Chief Scientific ... give the required acetyl compound , and a product was isolated which proved to be the diacetyl derivative . Later , it ...
Page 136
... give b . p . 68.80 ° , d 0 · 65940 , no 1 · 37321 , nь 1 · 37512 , ng 1 ... B. P. 124.5 ° / 760 mm .; M 114-22 ; no 1 · 39544 , nd 1 · 39743 , nr 1 ... give b . p . 125.80 ° , d 0 · 70197 , no 1.39512 , np 1 · 39727 , nr 1 · 40240 . Lek ...
... give b . p . 68.80 ° , d 0 · 65940 , no 1 · 37321 , nь 1 · 37512 , ng 1 ... B. P. 124.5 ° / 760 mm .; M 114-22 ; no 1 · 39544 , nd 1 · 39743 , nr 1 ... give b . p . 125.80 ° , d 0 · 70197 , no 1.39512 , np 1 · 39727 , nr 1 · 40240 . Lek ...
Page 137
... pressure ; there is slight decomposition at atmospheric pressure . B. p . 87 ° / 20 ... give b . p . 195 · 84 ° , d 0 · 74025 , n 。 1 · 41514 , nd 1 · 41727 , nƑ 1 ... b.p. 99-100 ° / 7 mm . , were obtained . After treatment with 4 - ml ...
... pressure ; there is slight decomposition at atmospheric pressure . B. p . 87 ° / 20 ... give b . p . 195 · 84 ° , d 0 · 74025 , n 。 1 · 41514 , nd 1 · 41727 , nƑ 1 ... b.p. 99-100 ° / 7 mm . , were obtained . After treatment with 4 - ml ...
Contents
The Ternary Systems NaSCNCa SCNH₂O KSCNCaSCNH₂O NHSCNCaSCNH₂O | 1 |
Rareearth Metal Oxides | 7 |
The Acetone Derivatives of Hexahydric Alcohols Part I Triacetone Mannitol and its Conversion | 13 |
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3′-pyridoacridine 4-dideuterobenzene absorption acetic acid acetone acridone active added alkali alkyl Amer amidine ammonia atoms bands benzene bimolecular boiling Calc carbinol CH₂ Chem Chemical chloride combination tones compound condensation cooled crude crystallised D.Sc decomp derivative deuterated benzenes deuterium dilute dissolved distilled dried effect ester ether ethyl alcohol experimental extracted filtered formed Found fraction fundamental frequencies gave give b. p. halides heated hexadeuterobenzene hydrochloric acid hydrochloride hydrogen hydrolysis infra-red spectrum Ingold iodide ionisation isolated ketone kg.-cals ligroin methanol method mixture molecule monodeuterobenzene neopentyl neopentyl bromide nitrate normal co-ordinates obtained oxide picrate potassium potassium carbonate praseodymium precipitate prepared prisms pyridine Raman spectrum reaction reagent rearrangement refluxed requires residue salt separated sodium carbonate sodium hydroxide solid soluble solution solvent spectra steric steric effect stirred substitution sulphate sulphuric acid symmetry class Table temperature washed yellow needles yield