Quarterly Journal of the Chemical Society of London, Part 1, Pages 1033-2076 |
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Page 1689
... solid was formed . After 24 hr . , triphosphonitrilic fluoride ( 0.93 g . , 3.7 mmoles ) was recovered by vacuum transfer . The white solid residue was sublimed ( 110 ° / 0-01 mm . ) to give N , P , F , 2SbF ( 2-76 g . , 78 % ) , a ...
... solid was formed . After 24 hr . , triphosphonitrilic fluoride ( 0.93 g . , 3.7 mmoles ) was recovered by vacuum transfer . The white solid residue was sublimed ( 110 ° / 0-01 mm . ) to give N , P , F , 2SbF ( 2-76 g . , 78 % ) , a ...
Page 1814
... solid ( B ) which was then further dried in a desic- cator . This procedure has been the only satisfactory way of obtaining solids A and B. Method ( c ) . When preparation ( b ) was repeated , but with first adding sufficient perchloric ...
... solid ( B ) which was then further dried in a desic- cator . This procedure has been the only satisfactory way of obtaining solids A and B. Method ( c ) . When preparation ( b ) was repeated , but with first adding sufficient perchloric ...
Page 1844
... solid - state spectrum , and this has been shown to be due to interaction of the oxygen with a neighbouring tungsten in the solid . The crystal structure 7 of WOCl consists of infinite chains of alternat- ing oxygen and tungsten atoms ...
... solid - state spectrum , and this has been shown to be due to interaction of the oxygen with a neighbouring tungsten in the solid . The crystal structure 7 of WOCl consists of infinite chains of alternat- ing oxygen and tungsten atoms ...
Contents
Dolcetti G See Peloso A 1506 | 1031 |
Structures of cyclic amides Part III Thio and selenolactams | 1033 |
Equilibria in solutions which contain a metal ion and an aminoacid | 1039 |
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¹H n.m.r. spectrum absorption acetaldehyde acetone acid adduct Amer anion aqueous atoms bands benzene bond bromine trifluoride calculated carbon catalyst cation Chem chemical Chemistry chloride cm.¹ co-ordination cobalt(II coefficients complexes compounds concentration configuration corresponding coupling constant crystals cyanide dehy gel dichloromethane dilute doublet electronic energy equation ethanol ether experimental Figure five-co-ordinate fluorine formation frequencies halide heat hydrogen hydrogen cyanide hydrolysis i.r. spectra Inorg iodide iodobenzene isomers k₁ kcal lactams ligand magnetic Mc./sec measured metal methyl mixture mmoles mole-¹ molecular molecule n.m.r. spectra nickel nickel(II nitric oxide nitrogen observed obtained octahedral orbital oxygen parameters phosphine phosphorus Phys plexes PMe,Ph potassium prepared present proton Raman reaction resonance room temperature sample scandium(III showed shown similar sodium solid solution solvent species structure sulphur Table thallium thio thiocyanate thiocyanogen thiolactams titration trans trimethylsilyl tris(trimethylsilyl values yellow