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absorption acetic acid acetone activity added addition alcohol alkaline Amer amount anhydride appeared aqueous atoms band benzene boiling bond Calc carbon carbon tetrachloride catalyst Chem chloride chloroform collected colourless complex compound concentrated constant containing cooled corresponding crystallised crystals derivatives described determined dilute dissolved distilled dried effect ester ethanol ether evaporated excess EXPERIMENTAL experiments extracted filtered formation formed Found fraction further gave give heated heated under reflux hydrochloric acid hydrogen hydrolysis indicated ions isolated ketone light petroleum material measurements metal method methyl minutes mixed mixture needles observed obtained oxide plates possible potassium precipitated prepared presence pressure prisms reaction reduced removed requires residue respectively salt separated showed shown similar sodium solid soluble solution solvent stirred structure substance sulphone sulphuric acid Table treated washed yellow yield