Journal of the Chemical SocietyThe Society., 1954 |
From inside the book
Results 1-3 of 79
Page xv
... sulphuric acid . EXPERIMENTAL Isolation of the Dilution Products . - The general method for isolating the salts was ... acid , and so on , as has already been explained in Part XIV ( loc . cit . ) . It was necessary , however , to take ...
... sulphuric acid . EXPERIMENTAL Isolation of the Dilution Products . - The general method for isolating the salts was ... acid , and so on , as has already been explained in Part XIV ( loc . cit . ) . It was necessary , however , to take ...
Page 273
... sulphuric acid , adding water , collecting the precipitate , and finally washing with acetic acid . It was then boiled for 10 min . with stannous chloride ( 2 g . ) in glacial acetic acid ( 20 c.c. ) . On the addition of water a deep ...
... sulphuric acid , adding water , collecting the precipitate , and finally washing with acetic acid . It was then boiled for 10 min . with stannous chloride ( 2 g . ) in glacial acetic acid ( 20 c.c. ) . On the addition of water a deep ...
Page 988
... sulphuric acid ( 6 ml . ) in glacial acetic acid ( 10 ml . ) . After 72 hr . at 10 ° no appreciable change was visible . This condensation was not further investigated as reaction at suitably low temperatures was very slow ...
... sulphuric acid ( 6 ml . ) in glacial acetic acid ( 10 ml . ) . After 72 hr . at 10 ° no appreciable change was visible . This condensation was not further investigated as reaction at suitably low temperatures was very slow ...
Contents
Organic | xv |
Magnetic Moments and Stereochemistry of Cobaltous Compounds | xv |
789Tetrahydro4 7sulphinylthionaphthen | 15 |
136 other sections not shown
Other editions - View all
Common terms and phrases
absorption spectra acetic acid acetic anhydride acetone acetyl added addition alcohol alkaline alumina aluminium Amer amine ammonia aqueous atom band benzaldehyde benzene boiling bond bromide Calc carbonate carbonyl Chem chloride chloroform chromatography colour colourless complexes compound concentrated cooled crystallised crystals cyanogen cyanogen chloride decomp derivatives diazotised dilute dissolved distilled dried eluted equiv ester ether evaporated extracted ferric filtered formed Found fraction gave give H₂O heated hydrobromic acid hydrochloric acid hydrogen hydrogen chloride hydrolysis infra-red isolated ketone ligand light petroleum b. p. liquid m. p. and mixed methanol methyl mixed m. p. mixture molecule needles nitrate obtained orbitals oxidation phenol phosphate potassium hydroxide precipitate prepared pyridine reaction refluxed Reprint Order requires residue room temperature salt separated sodium carbonate sodium hydroxide solid solution solvent spectrum stirring sulphate sulphide sulphone sulphuric acid Table washed yield