Journal of the Chemical SocietyThe Society., 1950 |
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Page 205
... acid in acetic anhydride ( Tuey , Chem . and Ind . , 1948 , · 766 ) , alternative methods of preparation were investigated . Acetyl or benzoyl nitrate has been used for selective ortho - nitration of organic compounds but their use is ...
... acid in acetic anhydride ( Tuey , Chem . and Ind . , 1948 , · 766 ) , alternative methods of preparation were investigated . Acetyl or benzoyl nitrate has been used for selective ortho - nitration of organic compounds but their use is ...
Page 207
... Acetic Anhydride and Copper Nitrate . - Benzaldehyde ( 12 g . ) and acetic anhydride ( 60 g . ) were stirred together , and 5 drops of sulphuric acid ( d 1 · 84 ) added to catalyse the formation of the diacetate . After a further 15 ...
... Acetic Anhydride and Copper Nitrate . - Benzaldehyde ( 12 g . ) and acetic anhydride ( 60 g . ) were stirred together , and 5 drops of sulphuric acid ( d 1 · 84 ) added to catalyse the formation of the diacetate . After a further 15 ...
Page 965
... acetic acid of the solid so obtained gave yellow micro - crystals of 4 : 7 ... anhydride ( 3 c.c. ) and concentrated sulphuric acid ( 0.2 c.c. ) , gave the ... acetic acid ( 50 c.c. ) was added to a boiling solution of 4 - nitro - 3 ...
... acetic acid of the solid so obtained gave yellow micro - crystals of 4 : 7 ... anhydride ( 3 c.c. ) and concentrated sulphuric acid ( 0.2 c.c. ) , gave the ... acetic acid ( 50 c.c. ) was added to a boiling solution of 4 - nitro - 3 ...
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Common terms and phrases
4-dione absorption acetic acid acetic anhydride acetone acetyl activity added alcohol alkaline Amer amine ammonia amylose anhydride atom benzene boiling bromide bromine trifluoride Calc carbon dioxide carbon tetrachloride catalyst CH₂ Chem chloride chloroform CO₂ colour colourless complex compound cooling corresponding crystallised crystals cyclisation D.Sc decomp derivatives diazomethane dilute dioxan dissolved distilled disulphide dried electron ester ethanol ether ethyl acetate ethylamine evaporated extracted filtered filtrate formed Found fraction gave give heated under reflux hydrochloric acid hydrogen chloride hydrolysis iodide isolated ketone light petroleum b. p. liquid m. p. and mixed metals method methyl minutes mixed m. p. mixture molecule needles nitrate obtained oxidation potassium precipitate prepared prisms pyridine Q-enzyme reaction reagent reduced requires residue room temperature salt separated sodium hydroxide solid soluble solution solvent sulphate sulphide sulphuric acid washed yellow yield