Quarterly Journal of the Chemical Society of London |
From inside the book
Results 1-3 of 82
Page 2374
... refluxed for 7 hr . ( liquid temp . 107 ° ) , to give y - benzylmethylamino - a - phenyl- butyric acid hydrochloride ( 2 · 3 g . , 65 % ) , m . p . 202 ° , and benzyl chloride ( 250 mg . , 18 % ) . In a similar hydrolysis , the crude ...
... refluxed for 7 hr . ( liquid temp . 107 ° ) , to give y - benzylmethylamino - a - phenyl- butyric acid hydrochloride ( 2 · 3 g . , 65 % ) , m . p . 202 ° , and benzyl chloride ( 250 mg . , 18 % ) . In a similar hydrolysis , the crude ...
Page 2375
... refluxed for 2 hr . , and yielded benzyl chloride ( 30 mg . , 14 % ) . Independent Synthesis of y - Benzylmethylaminobutyric Acid Hydrochloride . - Diethyl malonate ( 23.5 g . ) , then a solution of 2 - benzylmethylaminoethyl chloride ...
... refluxed for 2 hr . , and yielded benzyl chloride ( 30 mg . , 14 % ) . Independent Synthesis of y - Benzylmethylaminobutyric Acid Hydrochloride . - Diethyl malonate ( 23.5 g . ) , then a solution of 2 - benzylmethylaminoethyl chloride ...
Page 2885
... refluxed with hydrazine ( 1 c.c. ) and potassium hydroxide ( 600 mg . ) in ethanol ( 25 c.c. ) for 30 min .; ethylene glycol ( 20 c.c. ) was added , aqueous ethanol ( 28 c.c. ) removed by distillation , and the temperature raised to 196 ...
... refluxed with hydrazine ( 1 c.c. ) and potassium hydroxide ( 600 mg . ) in ethanol ( 25 c.c. ) for 30 min .; ethylene glycol ( 20 c.c. ) was added , aqueous ethanol ( 28 c.c. ) removed by distillation , and the temperature raised to 196 ...
Contents
2 4Trimethylpentane | 2082 |
Cinnolines Part XXXIV 5 6 and 7Hydroxy and 5 6 and 7Aminocinnolines | 2100 |
The Conductometric Evaluation of the Ionisation Functions of the Monohalogenoacetic | 2104 |
116 other sections not shown
Other editions - View all
Common terms and phrases
absorption acetic anhydride acetone acetyl added alcohol alkaline Amer ammonia atom band benzene boiling bromine Calc carbon carbonyl Chem chloride chloroform colour colourless compound concentrated cooled crystallised crystals decomp derivative diethyl dilute dioxide dissolved distilled dried eluted ester ethanol ethylene evaporated filtered fluoride formed Found fraction gave give glacial acetic acid H₂O heated hydrochloric acid hydrogen hydrogen bromide hydrogen chloride hydrolysis infrared isolated ketone lanthanons light petroleum b. p. liquid lithium aluminium hydride m. p. and mixed method methyl mixed m. p. mixture mole needles nickel nitrate nitric nitryl fluoride obtained oxidation oxygen peroxide potassium hydroxide precipitate prepared pressure prisms pteridine pyridine reaction reduction refluxed Reprint Order requires residue resin room temperature sodium hydroxide solid soluble solution solvent spectra spectrum structure sulphuric acid Table tube ultraviolet vacuo washed yellow yield