Journal of the Chemical SocietyThe Society., 1953 |
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Page 165
... preparation . The fifth sample ( no . 10 ) , prepared hydrothermally ( Part II , J. , 1951 , 2397 ) , gave a curve ( Fig . 2 ) which was not very different from the others at 100 ° and above , but showed a much lower water content at ...
... preparation . The fifth sample ( no . 10 ) , prepared hydrothermally ( Part II , J. , 1951 , 2397 ) , gave a curve ( Fig . 2 ) which was not very different from the others at 100 ° and above , but showed a much lower water content at ...
Page 187
... prepared from the corresponding bromo - compounds by a method slightly modified from that used by Bance , Barber , and Woolman ( J. , 1943 , 1 ) for the TABLE 1. ( p - X • C ̧H1 ) 2C ° CY • C ̧H1Z - þ . Dose Time Dose Time X Y Ꮓ ( mg ...
... prepared from the corresponding bromo - compounds by a method slightly modified from that used by Bance , Barber , and Woolman ( J. , 1943 , 1 ) for the TABLE 1. ( p - X • C ̧H1 ) 2C ° CY • C ̧H1Z - þ . Dose Time Dose Time X Y Ꮓ ( mg ...
Page 291
... prepared by Weger and Döring , Ber . , 1903 , 36 , 881 ) . Diphenyl - 3 - carboxylate ( the acid was prepared by oxidation of 3 - methyldiphenyl , obtained by Gomberg reaction on m - toluidine ) , soluble , blue needles ( Found : Cu ...
... prepared by Weger and Döring , Ber . , 1903 , 36 , 881 ) . Diphenyl - 3 - carboxylate ( the acid was prepared by oxidation of 3 - methyldiphenyl , obtained by Gomberg reaction on m - toluidine ) , soluble , blue needles ( Found : Cu ...
Contents
Internuclear Cyclisation Part VII The Synthesis of Some NitroNmethyl | 1 |
Synthesis of Polymethylnaphthalenes | 8 |
Kestose a Trisaccharide formed from Sucrose by Yeast Invertase | 24 |
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absorption acetic acid acetic anhydride acetone acetyl acidified added alcohol alkaline aluminium aluminium chloride Amer amine aqueous sodium atom benzene boiling bromine Calc carbon Chem Chim chloroform chromatographed colourless compound concentrated cooled crystallised crystals D.Sc decomp derivatives dilute dissolved distilled dried elution equiv ester ethanol ethyl acetate ethylene evaporated extracted with ether filtered filtrate formed Found fraction gave give m. p. H₂O heated hydrochloric acid hydrogen chloride hydrogen sulphate hydrolysis hydroxyl infra-red iodide isolated ketone light petroleum b. p. liquid lithium aluminium hydride m. p. and mixed method mixed m. p. mixture mole obtained oxidation oxidised pale yellow phosphorochloridate polyporenic potassium hydroxide precipitate prepared prisms pyridine reaction reduced refluxed requires residue room temperature salt sodium hydroxide solid soluble solution solvent spectra sulphuric acid ultra-violet washed yellow needles yield