Quarterly Journal of the Chemical Society of London, Volume 14, Pages 1885-2708

acetic acid acetic anhydride acetylation added afforded alcohol alkaline Amer amine anhydride aqueous aromatic Autoxidation azide benzene boiling bromine Calc carbon CH₂ Chem chloride chloroform chromatography cm.¹ colourless compound cooled crystallised cyanide cyclisation decomp derivatives diazotised dichloromethane dilute dimethyl distilled dried eluted epoxide ester ethanol ethyl acetate evaporated extracted with ether filtered filtrate Found fraction gave give heated under reflux hydrochloric acid hydrogen hydrolysis i.r. spectrum isolated isomer ketone light petroleum lithium aluminium hydride log ɛ m.p. and mixed mass spectrum methyl mixed m.p. mixture mmol mmoles mole n.m.r. spectrum needles nitrogen obtained oxide phenyl phosphate potassium prepared protons pyridine quinone reaction reagent requires residue room temperature salt silica gel sodium hydroxide solid solution solvent spectra stirred structure Table tetrahydrofuran triazine washed with water yellow yield