Journal of the Chemical SocietyThe Society., 1955 |
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Page 1404
... ethers , and related reactions , are now reported in detail . Anisole , phenetole , and phenyl isopropyl ether with lead tetra - acetate in acetic acid at 80 ° give the p - acetoxy - ethers : the yields are small , unchanged ether is ...
... ethers , and related reactions , are now reported in detail . Anisole , phenetole , and phenyl isopropyl ether with lead tetra - acetate in acetic acid at 80 ° give the p - acetoxy - ethers : the yields are small , unchanged ether is ...
Page 1679
... ether . It was collected and treated with an excess of aqueous ammonia , and the free base extracted with ether . Evaporation of the dried ether extract gave pure p - nitroso - N - isopropylaniline , bluish - green crystals of metallic ...
... ether . It was collected and treated with an excess of aqueous ammonia , and the free base extracted with ether . Evaporation of the dried ether extract gave pure p - nitroso - N - isopropylaniline , bluish - green crystals of metallic ...
Page 2015
... ether . To the Grignard reagent prepared from iodobenzene ( 5.57 ml . ) and magnesium ( 1-2 g . ) in ether ( 20 ml . ) , dioxan ( 6 ml . ) was added dropwise with stirring , and the resulting paste treated with a solution of the anhydro ...
... ether . To the Grignard reagent prepared from iodobenzene ( 5.57 ml . ) and magnesium ( 1-2 g . ) in ether ( 20 ml . ) , dioxan ( 6 ml . ) was added dropwise with stirring , and the resulting paste treated with a solution of the anhydro ...
Contents
By F SMITH and LILIAN M TURTON | 1045 |
The Constitution of Homolycorine and Lycorenine | 1066 |
The Photolysis of Acetaldehyde Part III The Reaction in the Presence of Nitric | 1076 |
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Common terms and phrases
acetic anhydride acetone acetyl acidified added alcohol alkali Amer ammonia aqueous sodium aqueous solution atom benzene boiling bromine Calc carbon Chem chloride chloroform chromatography colourless compound concentrated cooled crystallised from methanol decomp derivative dilute dimethyl dioxan dissolved distillation dried eluted ester ethanol evaporated EXPERIMENTAL filtered filtrate formed Found fraction gave give glacial acetic acid H₂O heated hydrochloric acid hydrogen chloride hydrolysis iodide isolated ketone light petroleum b. p. lithium aluminium hydride m. p. and mixed method methyl mixed m. p. mixture molecule naphthazarin nitric oxide nitrogen obtained oxide pale yellow picrylsulphonate potassium hydroxide precipitate prepared prisms pyridine reaction reduced pressure refluxed removed Reprint Order requires residue ring room temperature salt separated sodium hydroxide solid soluble solvent steam-bath stirred structure sulphide sulphone sulphuric acid titration values vouacapenate washed yellow needles yield