Quarterly Journal of the Chemical Society of London, Volume 1 |
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Page 543
... ( ethanol ) [ trans - bis ( dimethyl- arsino ) ethylene ] nickel ( 11 ) . A solution of nickel ( 1 ) chloride hexahydrate ( 1 · 0 g , 1 mol ) in ethanol ( 50 ml ) was deaerated by passage of nitrogen through it for 20 min . The ligand ...
... ( ethanol ) [ trans - bis ( dimethyl- arsino ) ethylene ] nickel ( 11 ) . A solution of nickel ( 1 ) chloride hexahydrate ( 1 · 0 g , 1 mol ) in ethanol ( 50 ml ) was deaerated by passage of nitrogen through it for 20 min . The ligand ...
Page 549
... ethanol ( 5 ml ) and sodium iodide ( 1 · 2 g ) in ethanol ( 5 ml ) . The reaction was then carried out as in ( b ) , by use of ethanol ( 50 ml ) , ether ( 20 ml ) , water , and the ligand mixture ( 1 · 8 g , 2 mol ) . The initial ...
... ethanol ( 5 ml ) and sodium iodide ( 1 · 2 g ) in ethanol ( 5 ml ) . The reaction was then carried out as in ( b ) , by use of ethanol ( 50 ml ) , ether ( 20 ml ) , water , and the ligand mixture ( 1 · 8 g , 2 mol ) . The initial ...
Page 859
... ethanol ( 10 ml ) was stirred under carbon monoxide at -5 ° for 4 h . The white precipitated complex was filtered from the cold solution and washed with cold ethanol and dried in vacuo ( ca. 0.08 g , 75 % ) . The dicarbonyl acyl and ...
... ethanol ( 10 ml ) was stirred under carbon monoxide at -5 ° for 4 h . The white precipitated complex was filtered from the cold solution and washed with cold ethanol and dried in vacuo ( ca. 0.08 g , 75 % ) . The dicarbonyl acyl and ...
Contents
Inorganic physical and theoretical chemistry | 1 |
Singlecrystal vibrational spectrum of tetrakisthioacetamido copper 1 chloride | 8 |
Allylic complexes of ruthenium | 16 |
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absorption acid Acta Cryst adduct Amer amine angles aqueous assigned ation bands benzene bond lengths boron boron trichloride calculated carbon atom carbonyl Chem chemical Chemistry chloride cm-¹ cm¯¹ cm¹ co-ordination cobalt(II complexes compounds concentration crystal cyanide diethyl ether electron energy equation ethanol ether experimental factors Figure filtered fluorides formation frequencies halide hydrogen i.r. spectra imidazole Inorg intensity ions isomers k₁ kcal ligand measured metal methyl methylene mixture mmol modes mol-¹ molecular molecule n.m.r. spectra nickel nitrogen Nujol observed obtained olefin orbital oxide oxygen atoms parameters peaks perovskite phosphine photolysis Phys platinum plexes prepared present protons pyridine radical Raman rate constants ratio reaction resonance room temperature sample similar sodium solid solution solvent species spectra spectrum structure studies symmetry Table tetrahydrofuran thermal thorium triplet vacuo values vibrations X-ray yellow yield