Quarterly Journal of the Chemical Society of London, Volume 19 |
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Page 3306
... gave , on separation , hydrogen chloride ( 0.45 mmol ) in a -196 ° trap ; trisilane ( 0-15 mmol ) in a - 126 ° trap ; and 2 - chlorotrisilane ( ca. 0 · 05 mmol ; identi- fied by its i.r. spectrum ) in a - 63 ° trap . Formation and ...
... gave , on separation , hydrogen chloride ( 0.45 mmol ) in a -196 ° trap ; trisilane ( 0-15 mmol ) in a - 126 ° trap ; and 2 - chlorotrisilane ( ca. 0 · 05 mmol ; identi- fied by its i.r. spectrum ) in a - 63 ° trap . Formation and ...
Page 3388
... gave 1- ( 2 - hydroxy- phenyl ) -3 - phenyl - 5- ( 2 - carboxyphenyl ) formazanatocopper ( II ) ( II ; X = O , Y = CO2 , R Ph ) ( 3-6 g . , 86 % ) ( Found : C , 56-4 ; H , 3-5 ; Cu , 14-8 ; N , 13-0 . Calc . for C20H14CuN4O3 : C , 56.9 ...
... gave 1- ( 2 - hydroxy- phenyl ) -3 - phenyl - 5- ( 2 - carboxyphenyl ) formazanatocopper ( II ) ( II ; X = O , Y = CO2 , R Ph ) ( 3-6 g . , 86 % ) ( Found : C , 56-4 ; H , 3-5 ; Cu , 14-8 ; N , 13-0 . Calc . for C20H14CuN4O3 : C , 56.9 ...
Page 3471
... gave less of ( Ib ) . ( c ) With [ Me , GeRu ( CO ) ] 2.1 A sealed tube containing MeSi2H ( 350 mg . , 2.8 mmoles ) and [ Me , GeRu ( CO ) ] 2 ( 250 mg . , 0.38 mmole ) in hexane ( 15 ml . ) was irradiated for 36 hr . Chromatography of ...
... gave less of ( Ib ) . ( c ) With [ Me , GeRu ( CO ) ] 2.1 A sealed tube containing MeSi2H ( 350 mg . , 2.8 mmoles ) and [ Me , GeRu ( CO ) ] 2 ( 250 mg . , 0.38 mmole ) in hexane ( 15 ml . ) was irradiated for 36 hr . Chromatography of ...
Contents
Inorganic physical and theoretical chemistry | 2963 |
Structure of radicals produced by yradiolysis Part I 3Methylpentyl 2methylpentyl and isopentyl | 2971 |
Structure and conformational analysis of coordination complexes Part II XRay crystal structure of cis | 2981 |
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absorption acetate acetonitrile acid Acta Cryst adducts Amer angles anion aqueous assigned axis band benzene bond lengths calculated carbon carbonyl cation chelate Chem Chemical chemical shifts Chemistry chloride cm-¹ cm¹ co-ordination cobalt complexes compounds copper atom copper(II correlation coupling crystal derivatives deuterium diethyl ether doublet electron energy equation experimental Figure formation frequency H₂O halide hydrogen hydrogen bonding i.r. spectra indium(III Inorg intensity interaction iron(III isomer kinetic ligand magnetic metal methanol methyl mixture mmol mmoles molecular molecule n.m.r. spectra nitrogen Nujol observed obtained orbital oxide oxygen parameters phosphite Phys plane prepared present protons pyridine Raman reaction resonance rhodium ring room temperature salts shift shows similar SnCl sodium solid solution solvent space group species spectra spectrum stretching mode structure studies symmetry Table trans transition triphenylphosphine values vanadium(IV vibrational yellow