Journal of the Chemical Society, Part 3, Pages 2489-3512The Society., 1964 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
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Page 2511
... cooled , giving a mixture of red and yellow crystals . This mixture was extracted with cold benzene , leaving the small amount of yellow crystalline material undissolved . The benzene extract was evaporated to dryness and the residue ...
... cooled , giving a mixture of red and yellow crystals . This mixture was extracted with cold benzene , leaving the small amount of yellow crystalline material undissolved . The benzene extract was evaporated to dryness and the residue ...
Page 2512
... cooled , and water added . The resultant precipitate gave trichloro ( pyridine ) bis ( tri - n - propylphosphine ) rhodium ( III ) as orange prisms ( 0-50 g . ) , m . p . 173-186 ° ( decomp . ) ( from ethanol ) ( Found : C , 45-15 ; H ...
... cooled , and water added . The resultant precipitate gave trichloro ( pyridine ) bis ( tri - n - propylphosphine ) rhodium ( III ) as orange prisms ( 0-50 g . ) , m . p . 173-186 ° ( decomp . ) ( from ethanol ) ( Found : C , 45-15 ; H ...
Page 2804
... cooled and poured into water , affording 5 - nitro - 2 - toluene - p- sulphonylbenzylidene diacetate ( 5 · 3 g . ) , m . p . 150 ° ( from acetic acid ) ( Found : C , 53.0 ; H , 4.35 ; N , 3.6 . C18H1 , NO , S requires C , 53-1 ; H , 4-2 ...
... cooled and poured into water , affording 5 - nitro - 2 - toluene - p- sulphonylbenzylidene diacetate ( 5 · 3 g . ) , m . p . 150 ° ( from acetic acid ) ( Found : C , 53.0 ; H , 4.35 ; N , 3.6 . C18H1 , NO , S requires C , 53-1 ; H , 4-2 ...
Contents
Fluorocarbohydrates Part VIII Formation of halogenoderivatives from | 2493 |
Steric influences in radical reactions Part I Benzyl radicals derived from cyclic | 2500 |
56dioisopropylidene | 2514 |
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absorption acetic acid acetone added adduct alcohol Amax Amer aqueous aromatic ation atom atomic orbitals band benzene bond bromide Calc carbon carbonyl CH₂ Chem chloroform chromatography cm.¹ complex compound concentrated cooled crystallised cyclic cyclohexane decomp decomposition dilute dioxide distilled dried electron elution ester ethanol ether ethyl acetate evaporated extracted filtered filtrate formation formed Found fraction gave give heated hydrochloric hydrogen hydrogen chloride hydrolysis hydroxide infrared infrared spectrum ionisation energies isolated isomer ketone kinetic light petroleum mechanism methyl mixed m. p. mixture mole molecular molecule nitrate nitric nitric oxide nitrogen Nujol obtained oxide oxime perchlorate petroleum b. p. polymer potassium potassium hydroxide prepared proton pyridine reaction rearrangement reduced refluxed requires residue room temperature salt sodium solid solution solvent spectra structure sulphuric acid Table thionyl chloride transition ultraviolet values Vmax yellow yield