Journal of the Chemical Society, Part 1The Society., 1965 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
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Results 1-3 of 80
Page 366
... heated under reflux at 180 ° ( bath temp . ) / 14 mm . for 6 hr . The tetralol ( 2 g . ) The fused mixture Dehydration of 7 - Methoxy - 1,1 - dimethyl - 2 - tetralol .- ( i ) Xanthate method . and potassium hydroxide ( 1 · 2 g . ) were ...
... heated under reflux at 180 ° ( bath temp . ) / 14 mm . for 6 hr . The tetralol ( 2 g . ) The fused mixture Dehydration of 7 - Methoxy - 1,1 - dimethyl - 2 - tetralol .- ( i ) Xanthate method . and potassium hydroxide ( 1 · 2 g . ) were ...
Page 552
... heated in boiling ethanol ( 7 ml . ) for 1 hr . The product ( 0 · 4 g . ) was obtained as above ( Found : C , 25-2 ; H , 2-75 ; As , 23.9 ; Br , 12-6 ; Re , 29.7 . C13H16As2BrO2Re requires C , 24.6 ; H , 2 · 5 ; As , 23.8 ; Br , 12.6 ...
... heated in boiling ethanol ( 7 ml . ) for 1 hr . The product ( 0 · 4 g . ) was obtained as above ( Found : C , 25-2 ; H , 2-75 ; As , 23.9 ; Br , 12-6 ; Re , 29.7 . C13H16As2BrO2Re requires C , 24.6 ; H , 2 · 5 ; As , 23.8 ; Br , 12.6 ...
Page 964
... heated at 40-45 ° for a further 2 hr . , and finally heated at 90-100 ° for hr . The acetic acid was distilled off and the residue distilled to give an almost colourless liquid ( 24-7 g . ) , b . p . 100-104 ° / 0.2 mm . ( lit. , 13 128 ...
... heated at 40-45 ° for a further 2 hr . , and finally heated at 90-100 ° for hr . The acetic acid was distilled off and the residue distilled to give an almost colourless liquid ( 24-7 g . ) , b . p . 100-104 ° / 0.2 mm . ( lit. , 13 128 ...
Contents
Selfassociation and hydration of phenol in carbon tetrachloride | 1 |
Reactions of ketones with oxidising agents Part II Acetoxylation of 11 and | 6 |
Thermodynamic functions of phosphorus pentabromide | 7 |
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absorption acetic acid acetone acetyl added alumina Amax Amer ammonia aqueous atoms band benzene boiling bond bromine Calc calculated carbon tetrachloride catalysis cation CH₂ Chem chloroform chromatography cm.¹ complex compound concentration coupling constants crystallised crystals derivatives dichloride dilute distilled dried effect eluted ester ethanol ether ethyl acetate evaporated EXPERIMENTAL extracted filtered filtrate fluoride formation formed Found fraction gave H₂O heated hydride hydrochloric acid hydrogen chloride hydrolysis hydroxide infrared infrared spectrum isobutene k₁ ketone laminarin light petroleum methyl mixed m. p. mixture mmoles mole molecular molecule mµ ɛ needles nitrogen observed obtained oxide peak perchlorate phenol Phys platinum potassium prepared present proton pyridine react reaction reagent reflux requires residue resin ring room temperature salt sample sodium sodium hydroxide solid solution solvent spectra structure sulphuric acid t-butyl Table values washed yield