Quarterly Journal of the Chemical Society of London, Pages 3324-4156 |
From inside the book
Results 1-3 of 68
Page 3215
... Solid 100 ° 2 hr . Me or Et 0 Solid 100 ° 98 % AcOH B. P. 9 hr . Me or Et 0 98 % AcOH * 98 % AcOH * B. P. B. P. 5 min . Me or Et 0.5 Solid * Solid † 100 5 hr . 15 min . Me or Et 0 Me or Et 0.15 100 5 hr . Me or Et 0 15 min . Me or Et ...
... Solid 100 ° 2 hr . Me or Et 0 Solid 100 ° 98 % AcOH B. P. 9 hr . Me or Et 0 98 % AcOH * 98 % AcOH * B. P. B. P. 5 min . Me or Et 0.5 Solid * Solid † 100 5 hr . 15 min . Me or Et 0 Me or Et 0.15 100 5 hr . Me or Et 0 15 min . Me or Et ...
Page 3563
... solid gave starting material ( 101 mg . ) , m . p . 189-192 ° . Recrystallisation from ethanol gave needles ( 94 mg . ) , m . p . and mixed m . p . 190—192 ° . ( e ) 3 - Chloro - 2 : 4 : 6 - trimethoxyacetophenone ( 100 mg . ) was ...
... solid gave starting material ( 101 mg . ) , m . p . 189-192 ° . Recrystallisation from ethanol gave needles ( 94 mg . ) , m . p . and mixed m . p . 190—192 ° . ( e ) 3 - Chloro - 2 : 4 : 6 - trimethoxyacetophenone ( 100 mg . ) was ...
Page 3630
... solid carbon dioxide - alcohol freezing bath . A film of solid styrene formed on the inner surface of the vessel and was shaken free from time to time . In this way , 250 ml . of a sludge of liquid and solid styrene were prepared ...
... solid carbon dioxide - alcohol freezing bath . A film of solid styrene formed on the inner surface of the vessel and was shaken free from time to time . In this way , 250 ml . of a sludge of liquid and solid styrene were prepared ...
Contents
ii | 2842 |
Catalytic hydrogenation | 2845 |
Garden J F and Thomson R H | 2851 |
137 other sections not shown
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Common terms and phrases
4-triazine absorption acetic acid acetic anhydride acetone acidified added alcohol alkali alkyl Amer amine aqueous sodium atom band benzene benzyl boiling bromine Calc carbonate carbonyl Chem chloroform chromatography CO₂H colourless compound concentration containing cooled crystallised cyclisation decomp derivative diethyl dilute dioxan dioxide diphenyl dissolved distilled dried eluted ester ethanol ethyl acetate evaporated filtered filtrate fluorene formation formed Found fraction gave give H₂O heated hydrochloric acid hydrogen chloride hydrolysis infrared iodide isatin isolated ketone lactone light petroleum b. p. lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture mole needles nitric acid nitrogen obtained oxidation perchloric phenyl potassium hydroxide precipitate prepared prisms pyridine reaction reagent reduced refluxed requires residue room temperature salt separated sodium hydroxide solid solution solvent spectra structure sulphuric acid Table titration washed yellow yield