Journal of the Chemical Society, Part 1The Society., 1947 |
From inside the book
Results 1-3 of 73
Page 96
... methyl alcohol in needles , m . p . 81-82 ° undepressed by admixture with the product from method ( a ) . The non - steam - volatile residue was a sandy coloured powder , which after a preliminary crystallisation from methyl alcohol ...
... methyl alcohol in needles , m . p . 81-82 ° undepressed by admixture with the product from method ( a ) . The non - steam - volatile residue was a sandy coloured powder , which after a preliminary crystallisation from methyl alcohol ...
Page 552
... methyl - 3 - pyridazone ( Ach , loc . cit . , gives m . p . 81 ° ) ; yield , 0 · 5 g . ( 3 · 3 % ) ( Found : C , 60 ... alcohol in colourless needles , m . p . alone or in admixture with 4 - chloro - 2 - phenyl - 6 - methyl - 3 ...
... methyl - 3 - pyridazone ( Ach , loc . cit . , gives m . p . 81 ° ) ; yield , 0 · 5 g . ( 3 · 3 % ) ( Found : C , 60 ... alcohol in colourless needles , m . p . alone or in admixture with 4 - chloro - 2 - phenyl - 6 - methyl - 3 ...
Page 669
... ( alcohol ) had m . p . 202-204 ° , dependent on rate of heating ( Found : C ... methyl- arsine used ) . A portion , recrystallised again , had m . p . 244 ... alcohol ; the product ( 1 · 8 g . ) had m . p . 143–147 ° ( effer . ) without ...
... ( alcohol ) had m . p . 202-204 ° , dependent on rate of heating ( Found : C ... methyl- arsine used ) . A portion , recrystallised again , had m . p . 244 ... alcohol ; the product ( 1 · 8 g . ) had m . p . 143–147 ° ( effer . ) without ...
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Common terms and phrases
acetic anhydride acetone acetyl added alkaline Amer amidine amine ammonia ammonium aqueous sodium atoms benzene boiling bromide Calc CH₂ charcoal Chem chloroform colourless needles compound concentrated hydrochloric acid cooled crystallised crystallised from alcohol crystals cyanide D.Sc decomp derivative diazotised dilute dissolved distilled dried ester experimental extracted with ether filtered filtrate formed Found fraction gave give m. p. H₂O heated hydrochloric acid hydrogen chloride hydrolysis iodide isolated light petroleum m. p. and mixed methanol Methiodide method methyl alcohol minutes mixed m. p. molecular molecule nitration nitric acid obtained oxidation pale yellow petroleum b. p. phenyl picrate polymer polymerisation potassium precipitate prepared prisms pyridine reduced pressure refluxed removed requires residue room temperature salt separated sodium carbonate sodium hydroxide sodium nitrite solid soluble solvent stirred structure substance sulphate sulphide sulphone sulphuric acid washed yellow needles yield