Journal of the Chemical Society, Part 2, Pages 1201-2488The Society., 1964 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
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Page 1257
... Acetonitrile at 59.8 ° . - These rates were measured with a polarimeter tube ( 1 , 4 dm . ) equipped with a jacket through which water at 59.8 ° , from the thermostat ( which was covered with a film of oil to minimise the evaporation of ...
... Acetonitrile at 59.8 ° . - These rates were measured with a polarimeter tube ( 1 , 4 dm . ) equipped with a jacket through which water at 59.8 ° , from the thermostat ( which was covered with a film of oil to minimise the evaporation of ...
Page 1260
... acetonitrile ) has the same configuration and optical purity as 1 - phenylethylthiouronium toluene - p - sulphonate with [ M20 342 in water ( or , with slightly less accuracy , [ M ] , 20 354 ° in acetonitrile ) ; and , more ...
... acetonitrile ) has the same configuration and optical purity as 1 - phenylethylthiouronium toluene - p - sulphonate with [ M20 342 in water ( or , with slightly less accuracy , [ M ] , 20 354 ° in acetonitrile ) ; and , more ...
Page 1263
... Acetonitrile at 59.8 ° . - Titrimetric procedure . The reaction solution was prepared from a weighed amount of the sulphonium salt and a standard solution of tetraethylammonium toluene - p - sulphonate in acetonitrile . Samples were ...
... Acetonitrile at 59.8 ° . - Titrimetric procedure . The reaction solution was prepared from a weighed amount of the sulphonium salt and a standard solution of tetraethylammonium toluene - p - sulphonate in acetonitrile . Samples were ...
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1-methylheptyl 1-phenylethyl bromide absorption acetic acid acetone acetonitrile adducts alcohol Amer amine anhydride aniline aqueous atom benzene bond Calc calculated carbon carboxyl Chem chloroform chromatography complex compounds concentration correlation crystallised cyclopropane derived diazomethane diphenylphosphinic dissociation constants distilled enol equation equilibrium constants ester ethanol ether experimental extracted fluorine formation Found fraction gave H₂O halides hydrazine hydrides hydrogen cyanide hydrolysis hydroxide infrared spectrum ionisation isomers k₁ k₂ kcal kinetic ligand methanolysis mixed m. p. mixture mmoles mole mole-¹ molecular molecules nitrogen nucleophilic o-complex obtained oleyl alcohol optical orbitals oxaloacetic acid oxidation oxygen peak phenols phosphate phosphine picryl potassium prepared proton pyridine rate coefficients rate constants reaction reflux requires residue rotation shown similar sodium solution solvent spectra structure substituted sulphide t-butyl methyl t-butyl peroxide Table tetracyanoethylene titration toluene-p-sulphonate values yield