Journal of the Chemical Society, Part 2, Pages 1201-2488The Society., 1964 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
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Page 1320
... mmoles ) was added to sodium periodate ( 0.64 g . , 3 mmoles ) in acetate buffer ( sodium acetate - acetic acid , 85 : 15 , v / v ) , and the pH adjusted to 6-7 by the addition of glacial acetic acid ( 0-25 ml . ) . Hippurhydroxamic ...
... mmoles ) was added to sodium periodate ( 0.64 g . , 3 mmoles ) in acetate buffer ( sodium acetate - acetic acid , 85 : 15 , v / v ) , and the pH adjusted to 6-7 by the addition of glacial acetic acid ( 0-25 ml . ) . Hippurhydroxamic ...
Page 1546
... mmoles ) reacted vigorously with methyl iodide ( 0.44 ml . , 4.75 mmoles ) in ether ( 15 ml . ) to give a white methiodide ( 1 · 279 g . , 99 % ) , m . p . 170 ° ( decomp . ) ( Found : I , 22.8 . C2H2INP2 requires I , 23.5 ...
... mmoles ) reacted vigorously with methyl iodide ( 0.44 ml . , 4.75 mmoles ) in ether ( 15 ml . ) to give a white methiodide ( 1 · 279 g . , 99 % ) , m . p . 170 ° ( decomp . ) ( Found : I , 22.8 . C2H2INP2 requires I , 23.5 ...
Page 1547
... mmoles ) with activated manganese dioxide ( 1 · 162 g . , 13.4 mmoles ) in benzene ( 35 ml . ) under reflux for 2 hr . After filtration and repeated extraction of the residual dioxide with acetone , a white solid ( 0 · 503 g . , 47 ...
... mmoles ) with activated manganese dioxide ( 1 · 162 g . , 13.4 mmoles ) in benzene ( 35 ml . ) under reflux for 2 hr . After filtration and repeated extraction of the residual dioxide with acetone , a white solid ( 0 · 503 g . , 47 ...
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1-methylheptyl 1-phenylethyl bromide absorption acetic acid acetone acetonitrile adducts alcohol Amer amine anhydride aniline aqueous atom benzene bond Calc calculated carbon carboxyl Chem chloroform chromatography complex compounds concentration correlation crystallised cyclopropane derived diazomethane diphenylphosphinic dissociation constants distilled enol equation equilibrium constants ester ethanol ether experimental extracted fluorine formation Found fraction gave H₂O halides hydrazine hydrides hydrogen cyanide hydrolysis hydroxide infrared spectrum ionisation isomers k₁ k₂ kcal kinetic ligand methanolysis mixed m. p. mixture mmoles mole mole-¹ molecular molecules nitrogen nucleophilic o-complex obtained oleyl alcohol optical orbitals oxaloacetic acid oxidation oxygen peak phenols phosphate phosphine picryl potassium prepared proton pyridine rate coefficients rate constants reaction reflux requires residue rotation shown similar sodium solution solvent spectra structure substituted sulphide t-butyl methyl t-butyl peroxide Table tetracyanoethylene titration toluene-p-sulphonate values yield