Journal of the Chemical Society, Part 2, Pages 1201-2488The Society., 1964 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
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Page 1222
... sulphide were the sulphoxide and the x - benzoyloxy - sulphide : RS CH2R ' RSO CH2R ' + RS.CHR ' • O • COPh t - Butyl methyl sulphide and benzoyl peroxide at 18 gave benzoic acid ( 48 % ) and benzoic anhydride , together with t - butyl ...
... sulphide were the sulphoxide and the x - benzoyloxy - sulphide : RS CH2R ' RSO CH2R ' + RS.CHR ' • O • COPh t - Butyl methyl sulphide and benzoyl peroxide at 18 gave benzoic acid ( 48 % ) and benzoic anhydride , together with t - butyl ...
Page 1251
... sulphide . Rotations for the halides [ EtSNa ] , Max . value from Halide α120 [ Halide ] . ap for sulphide this work Chloride Bromide - 29.36 ° 3.9 : 1 13.0 ° 32.4 ° -39.6 10.6 1 12.78 44.5 -37.67 12.26 44.1 Iodide - 60.2 13.46 64.2 4.1 ...
... sulphide . Rotations for the halides [ EtSNa ] , Max . value from Halide α120 [ Halide ] . ap for sulphide this work Chloride Bromide - 29.36 ° 3.9 : 1 13.0 ° 32.4 ° -39.6 10.6 1 12.78 44.5 -37.67 12.26 44.1 Iodide - 60.2 13.46 64.2 4.1 ...
Page 1639
... sulphide as yellow needles ( 5.4 g . ) ( from alcohol ) , m . p . 46 · 5 ° ( Found : C , 69-2 ; H , 4 · 7 ; N , 4 · 5 . C17H1NOS requires C , 69 · 1 ; H , 4 · 4 ; N , 4 · 7 % ) . 6 - Methyl - 9 - thia - 1,2 - benzofluorene ( II ; R Me ) ...
... sulphide as yellow needles ( 5.4 g . ) ( from alcohol ) , m . p . 46 · 5 ° ( Found : C , 69-2 ; H , 4 · 7 ; N , 4 · 5 . C17H1NOS requires C , 69 · 1 ; H , 4 · 4 ; N , 4 · 7 % ) . 6 - Methyl - 9 - thia - 1,2 - benzofluorene ( II ; R Me ) ...
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1-methylheptyl 1-phenylethyl bromide absorption acetic acid acetone acetonitrile adducts alcohol Amer amine anhydride aniline aqueous atom benzene bond Calc calculated carbon carboxyl Chem chloroform chromatography complex compounds concentration correlation crystallised cyclopropane derived diazomethane diphenylphosphinic dissociation constants distilled enol equation equilibrium constants ester ethanol ether experimental extracted fluorine formation Found fraction gave H₂O halides hydrazine hydrides hydrogen cyanide hydrolysis hydroxide infrared spectrum ionisation isomers k₁ k₂ kcal kinetic ligand methanolysis mixed m. p. mixture mmoles mole mole-¹ molecular molecules nitrogen nucleophilic o-complex obtained oleyl alcohol optical orbitals oxaloacetic acid oxidation oxygen peak phenols phosphate phosphine picryl potassium prepared proton pyridine rate coefficients rate constants reaction reflux requires residue rotation shown similar sodium solution solvent spectra structure substituted sulphide t-butyl methyl t-butyl peroxide Table tetracyanoethylene titration toluene-p-sulphonate values yield