Quarterly Journal of the Chemical Society of London, Part 1, Pages 1-1200 |
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Page 254
... mixture of ammonium formate ( 25 g . ) and propio- phenone ( 17 g . ) was slowly distilled until the b . p . of the liquid distilling reached 180 ° . The propiophenone layer of the distillate was returned to the flask and the ...
... mixture of ammonium formate ( 25 g . ) and propio- phenone ( 17 g . ) was slowly distilled until the b . p . of the liquid distilling reached 180 ° . The propiophenone layer of the distillate was returned to the flask and the ...
Page 256
... mixture of tetrahydrophenylquinoline ( 10.2 g . ) , methyl iodide ( 9 g . ) , acetone ( 50 ml . ) and sodium carbonate ( 7 g . ) was heated under reflux for 12 hr . The usual method of working - up gave 1,2,3,4 - tetrahydro - 1 - methyl ...
... mixture of tetrahydrophenylquinoline ( 10.2 g . ) , methyl iodide ( 9 g . ) , acetone ( 50 ml . ) and sodium carbonate ( 7 g . ) was heated under reflux for 12 hr . The usual method of working - up gave 1,2,3,4 - tetrahydro - 1 - methyl ...
Page 1095
... mixture of the four possible compounds . Me [ CH , ] gCO [ CHg ] CO , H , Me • [ CH , ] * CO [ CH , ] • CO [ CH ... mixture , the oxo - acid alone , and reference compounds in carbon tetrachloride and ether - carbon tetra- chloride ( 1 ...
... mixture of the four possible compounds . Me [ CH , ] gCO [ CHg ] CO , H , Me • [ CH , ] * CO [ CH , ] • CO [ CH ... mixture , the oxo - acid alone , and reference compounds in carbon tetrachloride and ether - carbon tetra- chloride ( 1 ...
Contents
Preparation and reactions of some oxoalkyliron complexes | 1 |
Developments in the theory of cationic polymerisation Part IV A general | 16 |
The lowfrequency infrared spectra of some complex halides of zinc cadmium | 26 |
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absorption acetic acid acetic anhydride alkaline aluminium aluminium chloride Amax Amer amine ammonia aqueous aromatic atom band benzene bond bromide Calc carbon CH₂ Chem chloride chloroform chromatography cm.¹ complex compound concentration coupling constants crystallised crystals decomp decomposition derivative dilute dimethyl dimethyl ether distilled dried Elution equation erythroaphins ester ethanol ether ethyl acetate evaporated EXPERIMENTAL extracted filtered fluoride formation Found fraction gave halides heated hydrochloric acid hydrogen hydrolysis infrared infrared spectra iodide K₁ ligand light petroleum lithium aluminium hydride log ɛ m. p. and mixed maltose method mixed m. p. mixture mole molecules nitrogen obtained oxidation oxygen phenyl picrate potassium precipitate prepared proton pyridine quinone reaction recrystallised refluxed requires residue resonance room temperature salt sample sodium hydroxide solution solvent spectrum structure substitution Table ultraviolet values washed yield