Journal of the Chemical SocietyThe Society., 1948 |
From inside the book
Results 1-3 of 71
Page 297
... mixture was diluted with water ( 45 c.c. ) and shaken vigorously , the aqueous layer separated , and amyl alcohol removed in steam . The residual amine was distilled from a bath at 160-170 ° with superheated steam . Distillation was ...
... mixture was diluted with water ( 45 c.c. ) and shaken vigorously , the aqueous layer separated , and amyl alcohol removed in steam . The residual amine was distilled from a bath at 160-170 ° with superheated steam . Distillation was ...
Page 629
... mixture was refluxed for 8 hours . The reaction mixture was diluted with excess of water , and worked up as for ethyl acetate , but without the washing with saturated brine . The yield of n - butyl acetate , b . p . 125 ° / 755 mm ...
... mixture was refluxed for 8 hours . The reaction mixture was diluted with excess of water , and worked up as for ethyl acetate , but without the washing with saturated brine . The yield of n - butyl acetate , b . p . 125 ° / 755 mm ...
Page 665
... mixture of 70 g . of silver fumarate , 52 g . of n - propyl bromide , and 60 ml . of benzene was refluxed for 13 hours and afforded 28 g . of ester , b . p . 110 ° / 5 mm . n - Butyl fumarate . A mixture of 70 g . of silver fumarate ...
... mixture of 70 g . of silver fumarate , 52 g . of n - propyl bromide , and 60 ml . of benzene was refluxed for 13 hours and afforded 28 g . of ester , b . p . 110 ° / 5 mm . n - Butyl fumarate . A mixture of 70 g . of silver fumarate ...
Contents
kilocals as the free energy difference contributed by the hyperconjugated methyl group | 373 |
SIR WILLIAM RAMSAY AND Ralph Forster LABORATORIES | 417 |
control of anionotropic rearrangement and of the significance of conjugation and hypercon | 440 |
Other editions - View all
Common terms and phrases
4-dideuterobenzene absorption spectrum acetic acid acetic anhydride acetone added alkaline Amer ammonia analcite aqueous sodium atoms bands benzene boiling bond bromine Calc carbon catalyst CH₂ chabazite Chem chloride chloroform colourless needles compound concentrated cooled corresponding crystallised from alcohol crystals cyanide D.Sc decomp derivative dilute dissolved distilled dried electronic origin energy ester ethanol ether evaporated excited extracted filtered filtrate fluorescence formed Found fraction fundamental frequencies gave give H₂O heated hexadeuterobenzene hydrochloric acid hydrogen hydrogen chloride hydrolysis Ingold isolated kcals ketone light petroleum method methyl alcohol mixed m. p. mixture molecule obtained oxidation peroxide phenol potassium potassium hydroxide precipitated prepared prisms pyridine reaction reduced pressure refluxed requires residue room temperature salt separated sodium hydroxide solid soluble solution solvent spectra structure sulphide sulphuric acid symmetry transitions unsaturated upper electronic upper-state vibration washed yellow needles yield