Quarterly Journal of the Chemical Society of London |
From inside the book
Results 1-3 of 71
Page 1183
... acetone with sodium iodide ( 30 g . ) at 125 ° for 12 hours . After removal of the sodium methanesulphonate the solution was evaporated to dryness and the product isolated as described above . Methanesulphonyl monoiodo- 1 : 4-3 6 ...
... acetone with sodium iodide ( 30 g . ) at 125 ° for 12 hours . After removal of the sodium methanesulphonate the solution was evaporated to dryness and the product isolated as described above . Methanesulphonyl monoiodo- 1 : 4-3 6 ...
Page 1535
... acetone 3429 Symmetry index . TEIT THAT Water Solubility . cm . -1 Symmetry index . Aq . NaOH 3443 3432 3440 3435 3422 3430 2.1 2.3 3448 3451 3453 2.12 2.70 Water 3448 2.79 Aq . acetone Acetone Acetone 3460 3476 3477 1.0 Aq . NaOH 3437 ...
... acetone 3429 Symmetry index . TEIT THAT Water Solubility . cm . -1 Symmetry index . Aq . NaOH 3443 3432 3440 3435 3422 3430 2.1 2.3 3448 3451 3453 2.12 2.70 Water 3448 2.79 Aq . acetone Acetone Acetone 3460 3476 3477 1.0 Aq . NaOH 3437 ...
Page 1707
... acetone , and did not react with phenylhydrazine or hydroxylamine . The monohydrochloride crystallised from acetone - ethanol ( 1 : 2 ) in needles , m . p . 251-252 ° ( Found : C1 , 10-4 . C1H2ON , Cl requires Cl , 10.8 % ) . Use of 21 ...
... acetone , and did not react with phenylhydrazine or hydroxylamine . The monohydrochloride crystallised from acetone - ethanol ( 1 : 2 ) in needles , m . p . 251-252 ° ( Found : C1 , 10-4 . C1H2ON , Cl requires Cl , 10.8 % ) . Use of 21 ...
Contents
C Allen J Bolton H C and Lewis | 860 |
Campbell N R and Hunt J H 956 960 | 863 |
Organic | 866 |
160 other sections not shown
Other editions - View all
Common terms and phrases
2-deoxy-D-galactose absorption acetic acid acetone added alcohol alkaline aluminium aluminium chloride Amer anhydride aqueous atoms bands benzene benzoate boiling bond bromide Calc carbonate catalytic CH₂ Chem chloroform colour colourless oil compound concentrated condensation cooled coronene corresponding crude crystallised crystals decomp derivative dibromide dilute dioxan diphenyl dissolved distilled dried ester ethanol ethyl ethylene evaporated extracted with ether filtered filtrate Found fraction gave give heated under reflux hydrocarbon hydrochloric acid hydrogen bromide hydrogen chloride hydrolysis interface iodide isolated ketone light petroleum b. p. lithium lithium aluminium hydride methiodide method minutes molecule needles obtained oxide phosphoric acid phosphoryl chloride phthalide picrate plates potassium precipitate prepared prisms pyridine reduction removed requires residue room temperature salt semicarbazone separated sodium hydroxide solid solution solvent structure sulphuric acid synthesis syrup tetralone titration washed yellow yield zinc