Journal of the Chemical Society, Part 4, Pages 3513-4668The Society., 1964 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
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Page 3850
... petroleum ( b . p . 40—60 ° ; 100 ml . ) to give a solid ( 10 · 1 g . ) m . p . 64–74 ° . Crystallisation from light petroleum ( b . p . 60–80 ° ; 50 ml . ) gave the mixture as flat micro- needles ( 8.0 g . ) , m . p . 65 ° , max ...
... petroleum ( b . p . 40—60 ° ; 100 ml . ) to give a solid ( 10 · 1 g . ) m . p . 64–74 ° . Crystallisation from light petroleum ( b . p . 60–80 ° ; 50 ml . ) gave the mixture as flat micro- needles ( 8.0 g . ) , m . p . 65 ° , max ...
Page 3851
... petroleum ( b . p . 60- 80 ° ) ] . Four crystallisations of the solid ( 0.15 g . ) from light petroleum ( b . p . 60-80 ° ) gave the epimer as needles ( 70 mg . ) , m . p . 154–155 ° ( Found : C , 19.5 ; H , 1.2 ; Cl , 69.35 ...
... petroleum ( b . p . 60- 80 ° ) ] . Four crystallisations of the solid ( 0.15 g . ) from light petroleum ( b . p . 60-80 ° ) gave the epimer as needles ( 70 mg . ) , m . p . 154–155 ° ( Found : C , 19.5 ; H , 1.2 ; Cl , 69.35 ...
Page 4581
... petroleum ( 30 ml . ) was added and left overnight in an ice - box to give crude linderene ( I ) ( 5.9 g . ) . The mother - liquor was evaporated in vacuo leaving a reddish - brown oil ( 52.1 g . ) . The residue ( 44 · 3 g . ) was ...
... petroleum ( 30 ml . ) was added and left overnight in an ice - box to give crude linderene ( I ) ( 5.9 g . ) . The mother - liquor was evaporated in vacuo leaving a reddish - brown oil ( 52.1 g . ) . The residue ( 44 · 3 g . ) was ...
Contents
4028 | 3507 |
Nucleophilic reactivity | 3513 |
Molecular polarisability Dipole moments molar Kerr constants and apparent | 3523 |
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absorption acetic acid acetic anhydride acetone acetoxylation acetyl added alcohol alkaline alumina aluminium Amer amine atoms band benzene benzyl bond bromide Calc carbon carbonyl chabazite Chem chloride chloroform chromatography cm.¹ compounds concentration crystals decomp diethyl diluted dimethylformamide diol dissolved distilled dried ester ethanol ethyl acetate evaporated EXPERIMENTAL extracted with ether filtrate formation Found fraction gave give heated hydrochloric acid hydrochloride hydrogen hydrolysis hydroxyl infrared iodide isomers K₁ ketone light petroleum lithium lithium aluminium hydride log ɛ m. p. and mixed mixed m. p. mixture mole molecules needles nitrate nitric acid nitrogen o-xylene obtained optical oxide oxygen petroleum b. p. phenol picrate potassium precipitated prepared proton pyridine rate constants reaction recrystallised refluxed requires residue room temperature salt sodium hydroxide solvent spectra spectrum stirred structure substitution sulphuric acid Table values washed yield