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acetic acid acid activity added addition alcohol alkyl appear aqueous assignment atoms band base benzene boiling bromide calculated carbon Chem chloride collected colourless combination complete compound concentrated constant containing cooled corresponding crude crystallised derivatives described determined dilute dissolved distilled dried effect energy ether ethyl evaporated excess experimental experiments extracted filtered formed Found fraction frequencies further gave give given heated hydrochloric acid hydrogen indicated infra-red intensity isolated ketone light mannitol material measured methanol method mixture molecule needles observed obtained oxide possible potassium precipitate prepared present pressure prisms pure Raman reaction rearrangement recorded reduced refluxed removed requires residue respectively salt separated showed shown similar sodium hydroxide solid solution solvent spectrum stirred structure substance substitution sulphuric acid symmetry Table temperature vibration washed yellow yield