Journal of the Chemical SocietyThe Society., 1955 |
From inside the book
Results 1-3 of 78
Page 3382
... acetic acid ( 25 c.c. ) was refluxed for 16 hr . with hydriodic acid ( 7 c.c .; d 1.7 ; freshly distilled from hypophosphorous acid ) . The mixture was diluted with water and extracted with ether , and the extract washed with sodium ...
... acetic acid ( 25 c.c. ) was refluxed for 16 hr . with hydriodic acid ( 7 c.c .; d 1.7 ; freshly distilled from hypophosphorous acid ) . The mixture was diluted with water and extracted with ether , and the extract washed with sodium ...
Page 3801
... acetic acid or benzene , which caused partial dissociation into the monobromide and bromine . ( ii ) A suspension of 2 ' - benzyl- thioazobenzene - 2 - sulphenyl bromide ( 1 g . ) in glacial acetic acid ( 100 c.c. ) was shaken with ...
... acetic acid or benzene , which caused partial dissociation into the monobromide and bromine . ( ii ) A suspension of 2 ' - benzyl- thioazobenzene - 2 - sulphenyl bromide ( 1 g . ) in glacial acetic acid ( 100 c.c. ) was shaken with ...
Page 4485
... acetic and concentrated hydrochloric acid . 1- and 2 - Nitrotriphenylene . - Nitric acid ( 70 % w / w ; 1.67 c.c. ) was added during 45 min . to triphenylene ( 6 · 0 g . ) in acetic anhydride ( 330 c.c. ) at 60 ° , and the mixture was ...
... acetic and concentrated hydrochloric acid . 1- and 2 - Nitrotriphenylene . - Nitric acid ( 70 % w / w ; 1.67 c.c. ) was added during 45 min . to triphenylene ( 6 · 0 g . ) in acetic anhydride ( 330 c.c. ) at 60 ° , and the mixture was ...
Contents
Alkenylation with Lithium Alkenyls Part IX Synthesis of Dimethylbutadiene PAGE | 3324 |
Alkenylation with Lithium Alkenyls Part XII Dihydronaphthyl and Indenyl | 3337 |
11dimethylcarbazoles | 3362 |
24 other sections not shown
Other editions - View all
Common terms and phrases
4-dinitrophenylhydrazone absorption acetic acid acetic anhydride acetone acetyl added alcohol aldehyde alumina Amer ammonia aqueous ethanol atoms band benzene boiling Braude bromide Calc carbonate Chem chloride chloroform chromatography colour compound concentrated cooled crystallised from ethanol crystals cyclohexanone decomp derivatives dilute dissolved distilled dried electrode eluted ester ethanol ether evaporated filtered filtrate formed Found fraction gave give m. p. heated hydrochloric acid hydrogen hydrolysis imidine infrared iodide isolated ketone light petroleum b. p. lithium lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture molecules nickel nitrobenzene nitrogen obtained oxide peroxide phenolic potassium hydroxide prepared prisms pyridine Raney nickel reaction recrystallized reduction refluxed Reprint Order requires residue room temperature salt semicarbazone silicon tetrachloride sodium hydroxide solid solution solvent spectra steric stirred substituents sulphate sulphuric acid Table values washed yellow yield