Journal of the Chemical SocietyThe Society., 1955 |
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Page 3918
... compound , m . p . 100-110 ° ( indefinite ) ( yield , 7.5 g . , 50 % ) , and some dark red resin ( Found : loss at 116 ° / 3—5 mm . , 10.5 . 2C1H1904N , CH . requires C.H. , 10.1 % ) . The toluene compound melted at 95-110 ° ( Found ...
... compound , m . p . 100-110 ° ( indefinite ) ( yield , 7.5 g . , 50 % ) , and some dark red resin ( Found : loss at 116 ° / 3—5 mm . , 10.5 . 2C1H1904N , CH . requires C.H. , 10.1 % ) . The toluene compound melted at 95-110 ° ( Found ...
Page 3964
... compound , C30H23N , m . p . 215 ° , was isolated in 28 % yield in addition to the phenylpyridines and tri- and tetra- phenylmethane . Huisgen and Nakaten ( loc . cit . ) also isolated this compound in the same yield from the products ...
... compound , C30H23N , m . p . 215 ° , was isolated in 28 % yield in addition to the phenylpyridines and tri- and tetra- phenylmethane . Huisgen and Nakaten ( loc . cit . ) also isolated this compound in the same yield from the products ...
Page 4291
... compound containing a functional group into the corresponding perfluoro - compound and ( b ) synthesis of the polyfluoro - compound from smaller molecules . The replacement of hydrogen by fluorine in a compound which already contains ...
... compound containing a functional group into the corresponding perfluoro - compound and ( b ) synthesis of the polyfluoro - compound from smaller molecules . The replacement of hydrogen by fluorine in a compound which already contains ...
Contents
Alkenylation with Lithium Alkenyls Part IX Synthesis of Dimethylbutadiene PAGE | 3324 |
Alkenylation with Lithium Alkenyls Part XII Dihydronaphthyl and Indenyl | 3337 |
11dimethylcarbazoles | 3362 |
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4-dinitrophenylhydrazone absorption acetic acid acetic anhydride acetone acetyl added alcohol aldehyde alumina Amer ammonia aqueous ethanol atoms band benzene boiling Braude bromide Calc carbonate Chem chloride chloroform chromatography colour compound concentrated cooled crystallised from ethanol crystals cyclohexanone decomp derivatives dilute dissolved distilled dried electrode eluted ester ethanol ether evaporated filtered filtrate formed Found fraction gave give m. p. heated hydrochloric acid hydrogen hydrolysis imidine infrared iodide isolated ketone light petroleum b. p. lithium lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture molecules nickel nitrobenzene nitrogen obtained oxide peroxide phenolic potassium hydroxide prepared prisms pyridine Raney nickel reaction recrystallized reduction refluxed Reprint Order requires residue room temperature salt semicarbazone silicon tetrachloride sodium hydroxide solid solution solvent spectra steric stirred substituents sulphate sulphuric acid Table values washed yellow yield