Journal of the Chemical SocietyThe Society., 1955 |
From inside the book
Results 1-3 of 33
Page 3402
... nitrobenzene 1 - amino- 4 - benzamidoanthraquinone had m . p . 287 ° ( Battegay and Bernhardt , Bull . Soc . chim ... nitrobenzene ( 600 c.c. ) for 24 hr . Recrystallisation from nitrobenzene gave a dark blue product ( Found : C , 76-7 ...
... nitrobenzene 1 - amino- 4 - benzamidoanthraquinone had m . p . 287 ° ( Battegay and Bernhardt , Bull . Soc . chim ... nitrobenzene ( 600 c.c. ) for 24 hr . Recrystallisation from nitrobenzene gave a dark blue product ( Found : C , 76-7 ...
Page 3404
Chemical Society (Great Britain). for 20 hr . in nitrobenzene ( 500 c.c. ) , gave a product ( 34 g . ) . Crystallisation from nitrobenzene ( 1.9 1. ) gave red minute needles ( 22 g . ) ( Found : C , 71-2 ; H , 2-7 ; N , 5.2 . C28H14O6N2 ...
Chemical Society (Great Britain). for 20 hr . in nitrobenzene ( 500 c.c. ) , gave a product ( 34 g . ) . Crystallisation from nitrobenzene ( 1.9 1. ) gave red minute needles ( 22 g . ) ( Found : C , 71-2 ; H , 2-7 ; N , 5.2 . C28H14O6N2 ...
Page 3542
... nitrobenzene ( 25 c.c. ) for 100 min . ( c ) Metal phthalocyanines . ( i ) [ With MARGARET WHALLEY ] Di - iminoisoindoline ( 0 · 2 g . ) and nickel chloride ( 0.2 g . ) were dissolved separately in hot formamide ( 2 · 5 , 12.5 c.c. ...
... nitrobenzene ( 25 c.c. ) for 100 min . ( c ) Metal phthalocyanines . ( i ) [ With MARGARET WHALLEY ] Di - iminoisoindoline ( 0 · 2 g . ) and nickel chloride ( 0.2 g . ) were dissolved separately in hot formamide ( 2 · 5 , 12.5 c.c. ...
Contents
Alkenylation with Lithium Alkenyls Part IX Synthesis of Dimethylbutadiene PAGE | 3324 |
Alkenylation with Lithium Alkenyls Part XII Dihydronaphthyl and Indenyl | 3337 |
11dimethylcarbazoles | 3362 |
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Common terms and phrases
4-dinitrophenylhydrazone absorption acetic acid acetic anhydride acetone acetyl added alcohol aldehyde alumina Amer ammonia aqueous ethanol atoms band benzene boiling Braude bromide Calc carbonate Chem chloride chloroform chromatography colour compound concentrated cooled crystallised from ethanol crystals cyclohexanone decomp derivatives dilute dissolved distilled dried electrode eluted ester ethanol ether evaporated filtered filtrate formed Found fraction gave give m. p. heated hydrochloric acid hydrogen hydrolysis imidine infrared iodide isolated ketone light petroleum b. p. lithium lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture molecules nickel nitrobenzene nitrogen obtained oxide peroxide phenolic potassium hydroxide prepared prisms pyridine Raney nickel reaction recrystallized reduction refluxed Reprint Order requires residue room temperature salt semicarbazone silicon tetrachloride sodium hydroxide solid solution solvent spectra steric stirred substituents sulphate sulphuric acid Table values washed yellow yield