Journal of the Chemical SocietyThe Society., 1955 |
From inside the book
Results 1-3 of 77
Page 3398
... residue II ) , but this is not readily obtained pure from preparations containing only small quantities . Larger yields were obtained from runs such as A3 in which the thiol re - circulated through the hot tube by increasing the flow of ...
... residue II ) , but this is not readily obtained pure from preparations containing only small quantities . Larger yields were obtained from runs such as A3 in which the thiol re - circulated through the hot tube by increasing the flow of ...
Page 3465
... Residue FeSO47H2O 260 H2O ( 500 ) Room 45 * 22.6 9.0 7.3 5.7 260 2N - H2SO , ( 500 ) 5 * 15.5 13-2 33 5.7 2.5 350 2N - H2SO ( 500 ) 45 * 19-0 11.6 6.0 250 2N - H2SO , ( 500 ) 50 ° 3.6 30 * 6.9 15.8 4.1 2.5 250 H2O ( 500 ) 0-5 45 * 23.8 ...
... Residue FeSO47H2O 260 H2O ( 500 ) Room 45 * 22.6 9.0 7.3 5.7 260 2N - H2SO , ( 500 ) 5 * 15.5 13-2 33 5.7 2.5 350 2N - H2SO ( 500 ) 45 * 19-0 11.6 6.0 250 2N - H2SO , ( 500 ) 50 ° 3.6 30 * 6.9 15.8 4.1 2.5 250 H2O ( 500 ) 0-5 45 * 23.8 ...
Page 3966
... residue ( 0 · 084 g . ) . ( d ) With nitrosoacetanilide ( France , Heilbron , and Hey , J. , 1940 , 369 ; 3.56 g./100 ml . of pyridine ) . The reagent was dissolved in pyridine ( 25 ml . ) which had previously been cooled to -20 ° , and ...
... residue ( 0 · 084 g . ) . ( d ) With nitrosoacetanilide ( France , Heilbron , and Hey , J. , 1940 , 369 ; 3.56 g./100 ml . of pyridine ) . The reagent was dissolved in pyridine ( 25 ml . ) which had previously been cooled to -20 ° , and ...
Contents
Alkenylation with Lithium Alkenyls Part IX Synthesis of Dimethylbutadiene PAGE | 3324 |
Alkenylation with Lithium Alkenyls Part XII Dihydronaphthyl and Indenyl | 3337 |
11dimethylcarbazoles | 3362 |
24 other sections not shown
Other editions - View all
Common terms and phrases
4-dinitrophenylhydrazone absorption acetic acid acetic anhydride acetone acetyl added alcohol aldehyde alumina Amer ammonia aqueous ethanol atoms band benzene boiling Braude bromide Calc carbonate Chem chloride chloroform chromatography colour compound concentrated cooled crystallised from ethanol crystals cyclohexanone decomp derivatives dilute dissolved distilled dried electrode eluted ester ethanol ether evaporated filtered filtrate formed Found fraction gave give m. p. heated hydrochloric acid hydrogen hydrolysis imidine infrared iodide isolated ketone light petroleum b. p. lithium lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture molecules nickel nitrobenzene nitrogen obtained oxide peroxide phenolic potassium hydroxide prepared prisms pyridine Raney nickel reaction recrystallized reduction refluxed Reprint Order requires residue room temperature salt semicarbazone silicon tetrachloride sodium hydroxide solid solution solvent spectra steric stirred substituents sulphate sulphuric acid Table values washed yellow yield