Journal of the Chemical Society, Part 5The Society., 1965 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
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Page 6301
... Filtrate F was acidified with 3N - hydrochloric acid , and the finely divided precipitate collected at 0 ° ( filtrate G ) . After being successively extracted with boiling dimethylformamide and ethanol , it formed a white crystalline ...
... Filtrate F was acidified with 3N - hydrochloric acid , and the finely divided precipitate collected at 0 ° ( filtrate G ) . After being successively extracted with boiling dimethylformamide and ethanol , it formed a white crystalline ...
Page 7273
... filtrate , on standing at 4o , deposited red crystals of the thione ( VI ) ( 0-22 g . ) , which after ... Filtrate . The filtrate was desalted electrolytically , during which a yellow precipitate separated . A portion of the desalted ...
... filtrate , on standing at 4o , deposited red crystals of the thione ( VI ) ( 0-22 g . ) , which after ... Filtrate . The filtrate was desalted electrolytically , during which a yellow precipitate separated . A portion of the desalted ...
Page 7347
... filtrate crystallised from aqueous acetonitrile at 2 ° , to yield the product ( 16 · 3 g . ) , m . p . 53—54 ° ; a further 2-3 g . were obtained by recrystallising the residue from the evaporated filtrate ( total yield , 85-5 ...
... filtrate crystallised from aqueous acetonitrile at 2 ° , to yield the product ( 16 · 3 g . ) , m . p . 53—54 ° ; a further 2-3 g . were obtained by recrystallising the residue from the evaporated filtrate ( total yield , 85-5 ...
Contents
ptolyl | 5785 |
The crystal structure of dipotassium bistrimethylenedinitramine nickelate11 | 5801 |
Coordination compounds having carboxylic esters as ligands | 5826 |
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absorption acetic acid acetic anhydride acetone Amer amine anhydride aqueous atoms band benzene benzyl bond borazocine boron bromide Calc carbon carbon tetrachloride carbonyl CH₂ Chem chloride chloroform chromatography cm.¹ complex compounds concentration constants crystallised decomp derivatives dilute dissolved distilled eluted ester ethanol ether ethyl acetate evaporated extracted filtered filtrate fluoride Found fraction gave give H₂O heated under reflux hydrochloric acid hydrogen hydrogen chloride hydrolysis hydroxide infrared infrared spectrum iodide isolated isomer ketone ligand light petroleum m. p. and mixed methyl mixed m. p. mixture mmoles mole molecule n.m.r. spectrum nitrogen obtained olefin optical oxazolone oxide peak perchlorate phenyl potassium prepared proton pyridine reaction requires residue ring room temperature salt showed sodium sodium hydroxide solid soluble solution solvent spectra structure sulphide sulphoxide sulphuric Table thionyl chloride vacuo values VIII yellow yield