Journal of the Chemical Society, Part 5The Society., 1965 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
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Page 6074
... gave the malonamide ( IIa ) in good yield . Cyclisation of this compound with sodium ethoxide gave a mixture of ( IIIa ) and its ethyl ester . A similar mixture was obtained by ring- closure of the methyl ester ( IIb ) with sodium ...
... gave the malonamide ( IIa ) in good yield . Cyclisation of this compound with sodium ethoxide gave a mixture of ( IIIa ) and its ethyl ester . A similar mixture was obtained by ring- closure of the methyl ester ( IIb ) with sodium ...
Page 6122
... gave an oil which gave a negative Beilstein test . The crude semicarbazone was cleaved readily on treatment with dioxan containing sulphuric acid ( 10 ml .; 40 % v / v ) . Dilution with water , and extraction with ether gave an oil ...
... gave an oil which gave a negative Beilstein test . The crude semicarbazone was cleaved readily on treatment with dioxan containing sulphuric acid ( 10 ml .; 40 % v / v ) . Dilution with water , and extraction with ether gave an oil ...
Page 6281
... gave a sparingly soluble sodium salt , which , when dissolved in water and acidified with acetic acid , gave ( B ) . Crystallis- ation of ( B ) from chloroform - light petroleum at room temperature gave rise to ( A ) , whereas ...
... gave a sparingly soluble sodium salt , which , when dissolved in water and acidified with acetic acid , gave ( B ) . Crystallis- ation of ( B ) from chloroform - light petroleum at room temperature gave rise to ( A ) , whereas ...
Contents
ptolyl | 5785 |
The crystal structure of dipotassium bistrimethylenedinitramine nickelate11 | 5801 |
Coordination compounds having carboxylic esters as ligands | 5826 |
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absorption acetic acid acetic anhydride acetone Amer amine anhydride aqueous atoms band benzene benzyl bond borazocine boron bromide Calc carbon carbon tetrachloride carbonyl CH₂ Chem chloride chloroform chromatography cm.¹ complex compounds concentration constants crystallised decomp derivatives dilute dissolved distilled eluted ester ethanol ether ethyl acetate evaporated extracted filtered filtrate fluoride Found fraction gave give H₂O heated under reflux hydrochloric acid hydrogen hydrogen chloride hydrolysis hydroxide infrared infrared spectrum iodide isolated isomer ketone ligand light petroleum m. p. and mixed methyl mixed m. p. mixture mmoles mole molecule n.m.r. spectrum nitrogen obtained olefin optical oxazolone oxide peak perchlorate phenyl potassium prepared proton pyridine reaction requires residue ring room temperature salt showed sodium sodium hydroxide solid soluble solution solvent spectra structure sulphide sulphoxide sulphuric Table thionyl chloride vacuo values VIII yellow yield