Journal of the Chemical Society, Part 5The Society., 1965 "Titles of chemical papers in British and foreign journals" included in Quarterly journal, v. 1-12. |
From inside the book
Results 1-3 of 71
Page 6056
... Iodide . - Triphenylphosphine ( 262 g . ) , 2 - iodoethanol ( 172 g . ) , and benzene ( 21. ) were refluxed together for 10 hr . , cooled , and filtered , to give 2 - hydroxy- ethyltriphenylphosphonium iodide ( 410 g . , 95 ...
... Iodide . - Triphenylphosphine ( 262 g . ) , 2 - iodoethanol ( 172 g . ) , and benzene ( 21. ) were refluxed together for 10 hr . , cooled , and filtered , to give 2 - hydroxy- ethyltriphenylphosphonium iodide ( 410 g . , 95 ...
Page 6348
... iodide , m . p . 256-257 ° ( effer . ) ( I.T. 250 ° ) from aqueous ethanol , and drying at 90 ° / 0-1 mm . ( Found ... iodide . The di - iodide dihydrate slowly separated as crystals , which when collected , triturated with water , and ...
... iodide , m . p . 256-257 ° ( effer . ) ( I.T. 250 ° ) from aqueous ethanol , and drying at 90 ° / 0-1 mm . ( Found ... iodide . The di - iodide dihydrate slowly separated as crystals , which when collected , triturated with water , and ...
Page 6349
... iodide for 2 hr . and evapor- ated to dryness ; the residue afforded the methiodide monohydrate , m . p . 218–221 ° , from ethanol with drying at 80 ° / 0 · 1 mm . ( Found : C , 50-3 ; H , 4 · 4 . C20H1ASI , H2O requires C , 50-2 ; H ...
... iodide for 2 hr . and evapor- ated to dryness ; the residue afforded the methiodide monohydrate , m . p . 218–221 ° , from ethanol with drying at 80 ° / 0 · 1 mm . ( Found : C , 50-3 ; H , 4 · 4 . C20H1ASI , H2O requires C , 50-2 ; H ...
Contents
ptolyl | 5785 |
The crystal structure of dipotassium bistrimethylenedinitramine nickelate11 | 5801 |
Coordination compounds having carboxylic esters as ligands | 5826 |
Copyright | |
146 other sections not shown
Other editions - View all
Common terms and phrases
absorption acetic acid acetic anhydride acetone Amer amine anhydride aqueous atoms band benzene benzyl bond borazocine boron bromide Calc carbon carbon tetrachloride carbonyl CH₂ Chem chloride chloroform chromatography cm.¹ complex compounds concentration constants crystallised decomp derivatives dilute dissolved distilled eluted ester ethanol ether ethyl acetate evaporated extracted filtered filtrate fluoride Found fraction gave give H₂O heated under reflux hydrochloric acid hydrogen hydrogen chloride hydrolysis hydroxide infrared infrared spectrum iodide isolated isomer ketone ligand light petroleum m. p. and mixed methyl mixed m. p. mixture mmoles mole molecule n.m.r. spectrum nitrogen obtained olefin optical oxazolone oxide peak perchlorate phenyl potassium prepared proton pyridine reaction requires residue ring room temperature salt showed sodium sodium hydroxide solid soluble solution solvent spectra structure sulphide sulphoxide sulphuric Table thionyl chloride vacuo values VIII yellow yield