Journal of the Chemical Society, Part 1The Society., 1959 |
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Page 121
... bromide 15 , 16 gives almost entirely the chlorohydrin ( VII ) and with tert . - butylmagnesium chloride is reduced to cis - 2 - chlorocyclohexanol , 17 gives a mixture of cis- and trans - 2 - chlorocyclohexanols on reduction by lithium ...
... bromide 15 , 16 gives almost entirely the chlorohydrin ( VII ) and with tert . - butylmagnesium chloride is reduced to cis - 2 - chlorocyclohexanol , 17 gives a mixture of cis- and trans - 2 - chlorocyclohexanols on reduction by lithium ...
Page 995
... bromide : NO , [ TiBr , ( NH , ) , ] * [ Ti ( NO ) , ( NH3 ) 3 ] 2+ Br The tensimetric studies at -36 ° show that almost 3 mol . of ammonium bromide but only 2.5 mol . of ammonium iodide are formed in the titanium ( IV ) bromide- and ...
... bromide : NO , [ TiBr , ( NH , ) , ] * [ Ti ( NO ) , ( NH3 ) 3 ] 2+ Br The tensimetric studies at -36 ° show that almost 3 mol . of ammonium bromide but only 2.5 mol . of ammonium iodide are formed in the titanium ( IV ) bromide- and ...
Page 1192
... bromide . results are discussed in relation to previous work on the decomposition of alkyl bromides . THE thermal decomposition of ethyl bromide has been extensively studied by Daniels and his co - workers . In a recent publication 1 in ...
... bromide . results are discussed in relation to previous work on the decomposition of alkyl bromides . THE thermal decomposition of ethyl bromide has been extensively studied by Daniels and his co - workers . In a recent publication 1 in ...
Contents
3Dioxa and 1 3 | 1 |
Triterpenoids Part LVII The oxidation of norfriedelanone with selenium dioxide | 38 |
2dichloro3 4epoxybutane and related compounds | 44 |
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absorption acetic acid acetone acetyl chloride added alcohol alkaline alumina Amer amine anhydride aqueous sodium atom band benzene boiling bond bromide Calc carbonyl CH₂ Chem chloroform chromatography complex compound concentrated cooled crystallised cyclohexene decomp derivative dilute dioxan distilled dried electron eluted epoxide ester ethanol evaporated excess extracted with ether filtered filtrate fluoride formation formed Found fraction gave give heated under reflux hydrochloric acid hydrogen chloride hydrolysis hydroxyl ibid infrared spectrum iodide isolated isomers ketone lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture mmole molecule needles nitrate nitrogen nitrous acid obtained olefin oxidation oxygen peroxide picrate potassium hydroxide precipitate prepared pyridine radicals reaction reagent reduced requires residue room temperature salt separated sodium hydroxide solid solution solvent spectra structure sulphuric acid Table tetrachloride triethylamine ultraviolet values washed yellow yield