Journal of the Chemical Society, Part 2The Society., 1959 |
From inside the book
Results 1-3 of 83
Page 1317
... excess of the acid chloride for 3 hr . at 70-80 ° with continuous stirring ( mercury seal ) . Then the benzene and the excess of acid chloride are distilled off under vacuum , and the residue is extracted with sodium carbonate solution ...
... excess of the acid chloride for 3 hr . at 70-80 ° with continuous stirring ( mercury seal ) . Then the benzene and the excess of acid chloride are distilled off under vacuum , and the residue is extracted with sodium carbonate solution ...
Page 1470
... excess . Assumptions ( 2 ) and ( 3 ) both give values higher than the equilibrium surface excess , but the values from assumption ( 2 ) [ Points ( 2 ) , Fig . 5 ] are in closest agreement with the true equilibrium value . The initial ...
... excess . Assumptions ( 2 ) and ( 3 ) both give values higher than the equilibrium surface excess , but the values from assumption ( 2 ) [ Points ( 2 ) , Fig . 5 ] are in closest agreement with the true equilibrium value . The initial ...
Page 1506
... excess of bromide ion . We have investigated further this reaction in methanol and water , so that the spectra could ... excess ( see Experimental section ) . 4.0 II FIG . 2. Absorption spectra of [ NEt , ] , [ PdBr1 ] : ( I ) in MeOH ...
... excess of bromide ion . We have investigated further this reaction in methanol and water , so that the spectra could ... excess ( see Experimental section ) . 4.0 II FIG . 2. Absorption spectra of [ NEt , ] , [ PdBr1 ] : ( I ) in MeOH ...
Contents
Potentially tautomeric pyridines Part II 2 3 and 4Acetamido and benz | 1317 |
ABEL E W and Wilkinson G 1501 | 1324 |
The second rapid step in the nucleophilic substitution of alkyl halides Part I | 1327 |
53 other sections not shown
Other editions - View all
Common terms and phrases
absorption acetic acid acetic anhydride acetone added alcohol alumina Amer amine anhydride anhydrous atom band benzene benzyl boiling bond bromide Calc carbon carboxylic CH₂ Chem chloride chloroform chromatography complex compound concentration constant crystals cyclic decomp derivatives dilute dioxan dissolved distilled dried elution ester ethanol ethyl acetate ethylene evaporated filtered formed Found fraction gave give H₂O halides heated hydrochloric acid hydrogen hydrogen chloride hydrolysis hydroxide infrared iodide ionic isolated ketone light petroleum b. p. lithium lithium aluminium hydride m. p. and mixed methyl mixed m. p. mixture mole molecular molecule needles nitrogen obtained oxide phenol phosphate picrate polymer potassium potassium hydroxide precipitate prepared prisms pyridine reaction reduced refluxed requires residue room temperature salt sodium hydroxide solid solvent spectra spectrum structure sulphate sulphuric acid Table tetrachloride values washed yellow yield