Quarterly Journal of the Chemical Society of London, Part 4, Pages 4613-5784 |
Contents
NO PAGE | 5064 |
NOTES | 5108 |
Double pinacoltype rearrangement leading to a 14diketone | 5123 |
7 other sections not shown
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absorption acetone added adduct Amer amine aqueous ascorbic acid atom band benzene bond bromide Calc carbon CH₂ Chem chloride chloroform chromatography circular dichroism cm.¹ complex components compound concentration crystallised cyanide decomp derivative dioxan distilled dried electron eluted ester ethanol ether ethyl acetate evaporated EXPERIMENTAL extracted Figure filtered filtrate Found fraction gave give halide heated hydride hydrogen hydrogen chloride hydrolysis infrared spectrum iodide irradiation isolated isomer ketone ligand light petroleum b. p. lithium aluminium hydride m. p. and mixed methyl mixed m. p. mmoles mole molecular molecule mucilage nitrogen obtained oxide peak perchloric phenyl potassium precipitate prepared proton pyridine rate constants reaction mixture reagent recrystallised reduction reflux requires residue resonance rhamnose ring room temperature sample showed sodium hydroxide solid solution solvent spectra stirred structure substituents Table thiocyanate ultraviolet vacuo values washed yield